Scientific American Supplement, No. 303, October 22, 1881Various
Science
Scientific American Supplement, No. 303, October 22, 1881
Various
Science -- Periodicals
for 20 minutes; I have, however, obtained very high vacua without using
this precaution.
During the process of exhaustion not more than one-half of the mercury
in the reservoir is allowed to run out, other wise when it is returned
bubbles of air are apt to find their way into the vacuum-bulb. In order
to secure its quiet entrance it is poured into a silk bag provided with
several holes. When the reservoir is first filled its walls for a day
or two appear to furnish air that enters the vacuum-bulb; this action,
however, soon sinks to a minimum and then the leakage remains quite
constant for months together.
_Measurement of the vacuum_.--The cylinder into which the gauge-tube
dips is first elevated by a box sufficiently thick merely to close the
gauge, afterwards boxes are placed under it sufficient to elevate the
mercury to the base of the measuring tube; when the mercury has reached
this point, thin boards and card-boards are added till a suitable
pressure is obtained. The length of the inclosed cylinder of air is
then measured with the cathetometer, also the height of the mercurial
"meniscus," and the difference of the heights of the mercurial columns
in A and B, figure 4. To obtain a second measure an assistant removes
some of the boxes and the cylinder is lowered by hand three or four
centimeters and then replaced in its original position. In measuring
really high vacua, it is well to begin with this process of lowering and
raising the cylinder, and to repeat it five or six times before taking
readings. It seems as though the mercury in the tube, B, supplies to the
glass a coating of air that allows it to move more freely; at all events
it is certain that ordinarily the readings of B become regular, only
after the mercury has been allowed to play up and down the tube a number
of times. This applies particularly to vacua as high 1/50,000,000 and to
pressures of five millimeters and under. It is advantageous in making
measurements to employ large pressures and small volumes; the correct
working of the gauge can from time to time be tested by varying the
relations of these to each other. This I did quite elaborately, and
proved that such constant errors as exist are small compared with
inevitable accidental errors, as, for example, that there was no
measurable correction for capillarity, that the calculated volume of the
"meniscus" was correct, etc. It is essential in making a measurement
that the temperature of the room should change as little as possible,
and that the temperature of the mercury in the cylinder should be at
least nearly that of the air near the gauge-sphere. The computation is
made as follows
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