Scientific American Supplement, No. 358, November 11, 1882Various
Science
Scientific American Supplement, No. 358, November 11, 1882
Various
Science -- Periodicals
This shows the advisability of utilizing all the direct light it
is possible to do, and thereby leaving as little as we can to be
accomplished by the reflector. When the sitter is arranged to the best
advantage at a window of ordinary size, fully exposed pictures can
generally be obtained with a portrait lens (full opening) in fairly good
light, on moderately sensitive plates, with one or two seconds' (or even
less) exposure. If a longer exposure than this be necessary, it
may fairly be assumed that the lighting has not been properly
managed.--_British Journal of Photography_.
* * * * *
A NEW METHOD OF PREPARING PHOTOGRAPHIC GELATINE EMULSION BY
PRECIPITATION OF THE BROMIDE OF SILVER.
By FRANZ STOLZE, Ph.D.
I consider the method of precipitation described below as far superior
to any other hitherto employed, particularly on account of its
infallible certainty. I began at first with a thirtieth of the whole
quantity of gelatine, and increased that quantity to a tenth without the
precipitate forming with greater difficulty. The salts were dissolved in
the usual quantity of water, the bromide of potassium was added to the
separately-dissolved gelatine, and both solutions cooled in iced water.
I soon found that even this was not necessary. I accelerated the
solution of the salts by vigorous agitation, so that the temperature
became so much lowered that, even after the addition of the warm
gelatine, it still remained low enough to give the precipitate when
mixed. The mixing took place gradually, all the usual precautionary
measures being observed; such as pouring the silver solution into No.
2 in small quantities at a time, and constantly stirring, and the
separation from the mother lye was complete.
The formula according to which I worked latterly was as follows:
SOLUTION I.
Nitrate of silver...................... 463 grains.
Water................................... 16¾ ounces.
SOLUTION II.
Bromide of potassium................... 355 grains.
Iodide of potassium..................... 15 grains.
Gelatine................................ 46 grains.
Water................................... 16¾ ounces.
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