Sapotiretin is an amorphous compound, insoluble in water, very soluble in alcohol, less soluble in chloroform, insoluble in ether. Below is the result of its analysis: Calculated for Found. C_{17}H_{32}O_{10}. I. II. C 51.52 51.51 51.20 H 8.08 8.19 8.34 --_Amer. Chem. Jour._ * * * * * DETECTION OF PEANUT OIL IN OLIVE OIL. Holde, after a careful trial of the various processes for detecting the above adulteration, gives the preference to Renard's, which he describes as follows: Ten grms. of the suspected oil, after being saponified, and the fatty acids separated by hydrochloric acid, are dissolved in 90 per cent. alcohol, and precipitated by sugar of lead. The oleate of lead is separated by ether, and the residuum, consisting of palmitic and arachic acids, is decomposed by hydrochloric acid. The fatty acids are dissolved, with the aid of heat, in 50 c.c. of 90 per cent. alcohol. The arachic acid which separates after cooling is filtered out and washed, first with 90 per cent. and afterward with 70 per cent. alcohol. It is then dissolved in hot alcohol, and the solution evaporated in a weighed saucer. The weight of the residuum, after taking into account the acid dissolved in the alcohol, equals the whole amount of arachic acid contained in the oil; the melting point of this residuum should be 70 deg. to 71 deg. C. With this process the author has always been successful; but when the olive oil contains not more than 5 to 10 per cent. of peanut oil, it is necessary to make the test with 40 grms. of the former, otherwise the melting point of the arachic acid cannot be estimated. Furthermore, the acids which are separated from the lead salt by hydrochloric acid must be recrystallized repeatedly with 90 per cent. alcohol, until the melting point ceases to rise, in case the latter is not found to exceed 70 deg. C. at the first estimation. When peanut oil is present, the melting point will always be above 70 deg..--_Chem. Zeit._ * * * * * HYDROXYLAMINE. Free hydroxylamine, NH_{2}OH, has been isolated by M. Lobry de Bruyn, and a preliminary account of its mode of preparation and properties is published by him in the current number of the _Recueil des travaux chimiques des Pays-Bas_ (1891, 10, 101). The manner in which the free base was obtained was briefly as follows. About a hundred grammes of hydroxylamine hydrochloride, NH_{2}OH.HCl, were dissolved in six hundred cubic centimeters of warm methyl alcohol. To this solution a quantity of sodium dissolved in methyl alcohol was added, in such proportion that the hydrochloride of hydroxylamine was present in slight excess over and above that required to convert it to sodium chloride. After deposition of the separated sodium chloride the solution was decanted and filtered.