Scientific American Supplement, No. 841, February 13, 1892Various
Science
Scientific American Supplement, No. 841, February 13, 1892
Various
Science -- Periodicals
Crystals of iodine dissolve instantly in contact with it, with
evolution of a gas and considerable rise of temperature. Bromine
reacts with violence, a gas again being explosively evolved and
hydrobromic acid formed. The nature of the gas evolved is now
undergoing investigation. A letter from M. Lobry de Bruyn appears in
the number of the _Chemiker Zeitung_ for October 31, warning those who
may attempt to prepare free hydroxylamine by the above method that it
is a dangerously explosive substance when warmed to a temperature of
80 deg.-100 deg.. Upon warming a flask containing the free solid base upon a
water bath a most violent explosion occurs. A spontaneous
decomposition appears to set in about 80 deg., and even in open vessels
the explosion is very violent. Care must also be taken during the
fractional distillation of the concentrated solution in methyl alcohol
to cool the apparatus before changing the receiver, as if air is
admitted while the retort is heated the experiment ends with an
explosion.--_Nature_.
* * * * *
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Public-domain text, read in full here on John Shaqi.
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