If the analysis of the tea-ash is referred to it will be noted that more
than one-half of it should be soluble in water, so that for all
practical purposes a complete analysis is not requisite, a determination
of the ratio of _soluble_ to _insoluble_ parts of the ash being
sufficient. Such a determination is made by boiling the ash several
times with a little water, filtering and washing the residue in the
filter, drying the precipitate, igniting and weighing it. The weight of
the insoluble part of the ash may then be subtracted from the weight of
the entire ash, in which manner both the percentage of the soluble and
insoluble ash will be conveniently arrived at, in which case the
following determination of the percentage of “soluble” and “insoluble
ash” in 100 parts of spurious leaves and pure tea when completely dried
will be of interest here:—
Kind of Leaf. Soluble Ash. Insoluble Ash.
Ash, 3.19 7.48
Plum, 5.66 4.24
Willow, 4.16 5.18
Teas of commerce, 3.55 2.47
Proving that in spurious leaves the ratio of soluble or insoluble ash is
very different from what it is in genuine tea-leaves, and that an ash of
such composition cannot be very soluble in water.
Peligot has also pointed out that tea leaves differ from other leaves by
their extraordinary richness in nitrogen, the prepared leaf being by the
process of curing rendered still more nitrogenous than the raw or spent
leaves, the former averaging, according to his experiments, 6 per cent.
of nitrogenous matter, and the latter 4.37, so that if the tea-leaf be
unique in containing such a high percentage of nitrogen, it is obvious
that a determination of nitrogen in tea may also be useful as a method
of identification.
The tea-extract also yields a comparatively large quantity of ammonia
when it is boiled with potash or permanganate of potash, and it is
probable that this characteristic may also prove very valuable in the
testing of tea. A solution containing about 10 per cent. of solid
potash, free from ammonia and nitrogenous matter is required for the
purpose, and easily obtained. So that a deficiency of theine, a
deficiency of nitrogen, and a deficiency of ammonia are all indicative
of the presence of foreign leaves in tea.
SPENT OR EXHAUSTED LEAVES IN TEA
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