The art of glass-blowing : $b or Plain instructions for making the chemical and philosophical instruments which are formed of glassDanger, T.-P.
Science
The art of glass-blowing : $b or Plain instructions for making the chemical and philosophical instruments which are formed of glass
Danger, T.-P.
Glass blowing and working
GRADUATION OF GAS JARS, TEST TUBES, &C.--If the tube is regular in the
bore, close one end, either by sealing it at the lamp, or by inserting
a cork, and pour into the interior two or three small and equal
portions of mercury, in order to have an opportunity of observing the
irregularities produced by the sealed part. Take care to mark, with a
writing diamond, the height of the mercury, after the addition of each
portion. When equal portions of mercury are perceived to fill equal
spaces, take with the compass the length of the last portion, and mark
it successively along the side of the tube, where you must previously
trace a line parallel to its axis.
For tubes which are irregular in the bore, and where equal lengths
indicate unequal capacities, it is necessary to continue the graduation
in the same manner that you commenced it--that is to say, to fill the
tubes by adding successively many small and equal portions of mercury,
and marking the height of the metallic column after every addition.
These divisions will of course represent parts of an ounce or of a
cubic inch according to the measure which you make use of. When you
have thus traced on the tube a certain number of equal parts, you can,
by means of the compasses, divide each of them into two other parts of
equal length. The first divisions being very close to one another, the
small portion of tube between every two may be considered without much
risk of error as being sensibly of equal diameter in its whole extent.
When the tube which you desire to graduate is long and has thin sides,
it would be difficult to fill it with mercury without running the risk
of seeing it break under the weight of the metal. In this case, you
must use water instead of mercury.
Bell-glasses of large dimensions are graduated by filling them with
water, placing them in an inverted position on a smooth and horizontal
surface, which is slightly covered with water, and passing under them
a series of equal measures of air. But it is then necessary to operate
constantly at the same temperature and under the same atmospheric
pressure, because air is very elastic and capable of being greatly
expanded.
In all cases, tubes, bell-glasses, &c. ought to be held in a position
perfectly vertical. The most convenient measure is a dropping-tube,
on the stalk of which a mark has been made, or a small piece of tube,
sealed at one end, and ground flat at the other; the latter can be
accurately closed by a plate of glass.
The marks which are traced on tubes being generally very close to one
another, you facilitate the reading of the scale by giving a greater
length to those marks which represent every fifth division, and by
writing the figures merely to every tenth division. See pl. 4, fig. 8.
The number of divisions is somewhat arbitrary; nevertheless, 100, 120,
360, 1000, are divisions which, in practice, offer most advantages.
* * * * *
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