The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.Piesse, G. W. Septimus (George William Septimus)
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The Art of Perfumery, and Methods of Obtaining the Odors of Plants: With Instructions for the Manufacture of Perfumes for the Handkerchief, Scented Powders, Odorous Vinegars, Dentifrices, Pomatums, Cosmetics, Perfumed Soap, Etc., to which is Added an Appendix on Preparing Artificial Fruit-Essences, Etc.
Piesse, G. W. Septimus (George William Septimus)
Cosmetics; Perfumes
For the preparation of the essence of pine-apple, one pound of this
ether is dissolved in 8 or 10 pounds of alcohol. 20 or 25 drops of this
solution is sufficient to give to one pound of sugar a strong taste of
pine-apple, if a little citric or tartaric acid has been added.
_Pear-oil._--This is an alcoholic solution of acetate of amyloxide, and
acetate of ethyloxide. For its preparation, one pound of glacial acetic
acid is added to an equal weight of fusel-oil (which has been prepared
by being washed with soda and water, and then distilled at a temperature
between 254 deg. and 284 deg. Fahr.), and mixed with half a pound of sulphuric
acid. The mixture is digested for some hours at a temperature of 254 deg.,
by which means acetate of amyloxide separates, particularly on the
addition of some water. The crude acetate of amyloxide obtained by
separation, and by the distillation of the liquid to which the water has
been added, is finally purified by being washed with soda and water.
Fifteen parts of acetate of amyloxide are dissolved with half a part of
acetic ether in 100 or 120 parts of alcohol; this is the essence of
pear, which, when employed to flavor sugar or syrup, to which a little
citric or tartaric acid has been added, affords the flavor of bergamot
pears, and a fruity, refreshing taste.
_Apple-oil_ is an alcoholic solution of valerianate of amyloxide. It is
obtained impure, as a by product, when for the preparation of valerianic
acid, fusel-oil is distilled with bichromate of potash and sulphuric
acid. It is better prepared in the following manner:--For the
preparation of valerianic acid, 1 part of fusel-oil is mixed gradually
with 3 parts of sulphuric acid, and 2 parts of water added. A solution
of 2-1/4 parts of bichromate of potash, with 4-1/2 parts of water, is
heated in a tubulated retort, and into this fluid the former mixture is
gradually poured, so that the ebullition is not too rapid. The
distillate is saturated with carbonate of soda, and warmed, when a
solution of 3 parts of crystallized carbonate of soda, 2 parts of strong
sulphuric acid, diluted with an equal quantity of water, are added. The
valerianic acid separates as an oily stratum.
One part, by weight, of pure fusel-oil is carefully mixed with an equal
weight of sulphuric acid. The cold solution is added to 1-1/4 parts of
the above valerianic acid; the mixture is warmed for some minutes (not
too long or too much) in a water-bath, and then mixed with a little
water, by which means the impure valerianate of amyloxide separates,
which is washed with water and carbonate of soda. For use as an essence
of apples, one part of this valerianate of amyloxide is dissolved in 6
or 8 parts of alcohol.
* * * * *
VOLATILE OIL OF GAULTHERIA PROCUMBENS.
BY W. BASTICK.
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