The Dyeing of Cotton Fabrics: A Practical Handbook for the Dyer and StudentBeech, Franklin
Science
The Dyeing of Cotton Fabrics: A Practical Handbook for the Dyer and Student
Beech, Franklin
Dyes and dyeing -- Cotton
=Preparation of diazotised paranitroaniline.=--Take 1 lb.
paranitroaniline, mix with 1 gallon boiling water and 1 quart
hydrochloric acid, stir well, when the paranitroaniline will dissolve
the solution may if necessary be assisted by a little heat. Now add
1-1/2 gallons of cold water, and set aside to cool, when the
hydrochloride of paranitroaniline will separate out in the form of fine
crystals; when the mixture is quite cold (it cannot be too cold) there
is added 1/2 lb. sodium nitrite dissolved in 1/2 gallon cold water, stir
well for fifteen to twenty minutes, by the end of which time the
paranitroaniline will have become fully diazotised, cold water is added
to bring up the volume of the mixture to 10 gallons. This stock bath
well prepared and kept in a cool, dark place will keep good for three to
four weeks. This bath contains 1 lb. of paranitroaniline in 10 gallons,
and it is a good rule to allow 1/2 lb., or 5 gallons of this stock bath
to each pound of dye-stuff used in dyeing the ground colour to be
developed up.
To prepare the coupling bath there is taken 5 gallons of the stock bath,
1 lb. sodium acetate with sufficient water for each 1 lb. of dye that
has been used.
This bath is used cold, and the cotton is worked in it for half an hour,
then it is taken out, washed well and dried.
Nitrazol C is a ready prepared diazotised paranitroaniline in a powder
form which keeps well if stored in a dry place. The method of using is
to take 8 lb. Nitrazol C, stir into a paste with water and then add this
paste to the coupling bath, together with 2 lb. soda and 3/4 lb. acetate
of soda. This bath is used cold and the dyed cotton is immersed in it
for half an hour, then taken out, well washed and dried.
The quantity of Nitrazol C given will suffice for all shades dyed with
from 2 to 4 per cent, of dye-stuff, but when paler shades are dyed,
using less than say 1/2 per cent. of dye-stuff, about 4 lb. Nitrazol C,
with the soda and acetate of soda in proportionate quantities, may be
used.
Azophor red P N is also a preparation of diazotised paranitroaniline in
the form of a dry powder which keeps well.
To prepare the coupling bath there is taken 2 lb. of Azophor red P N,
which is dissolved in water and added to the bath along with 1 lb.
acetate of soda. The dyed goods are worked in the cold bath for half an
hour, then taken out, well washed and dried.
The quantities given are sufficient for shades dyed with 2 to 4 per
cent. of dye-stuff; for weaker shades half the quantities may be taken.
Benzo-nitrol developer is sold in the form of a yellow paste. To use it
take 5 lb., stir into a smooth paste with water, then add to the
coupling bath. There is then added 3 pints of hydrochloric acid, with
some stirring. Allow to stand for half an hour, add 1-1/2 lb. acetate of
soda and 6-1/2 oz. soda, when the bath is ready for use. The cotton is
entered and worked for half an hour, then lifted out, washed and dried.
Public-domain text, read in full here on John Shaqi.
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