The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
When steam is utilised to extract dye-woods these defects are
removed. A burnt extract is not to be feared, and a small quantity of
water is sufficient to extract the colouring matter completely. The
apparatus illustrated in Fig. 37 is very suitable for the extraction
of dye-woods, and in general for obtaining vegetable extracts. The
extraction vessel is pear-shaped, its two hollow axes move in hollow
bearings. Thus it may be turned upside down, and steam and water can be
introduced into the interior through the axes, which are connected with
the pipes, E, W, and R. The opening at the pointed end of the pear is
closed by the screw, S; through it the substances to be extracted are
introduced. In the lower portion of the vessel is a sieve upon which
the materials are spread out. The opening of the pipe connected with E
and W is below the sieve.
[Illustration: FIG. 37.]
The process is commenced by introducing the materials through the
upper opening, fastening the cover down steam-tight by the lever,
B, and the screw, S, and then running in water through W until it
flows out through the lower of the two narrow pipes which are shown
somewhat paler in the shaded portion of the drawing. All the taps are
then closed with the exception of that on the upper of the two small
pipes. By opening the cock on R steam is led in. As a rule, steam at a
low pressure is used, not more than half an atmosphere. The contents
begin to boil in 15 to 30 minutes, steam then issues from the open
tap. According to the nature of the material to be extracted, boiling
is continued from 40 to 60 minutes. The side tap is then closed, and
the tap on the pipe E opened. The pressure of the steam now forces the
liquid up the pipe E; the pressure of half an atmosphere is sufficient
to raise it about 4 metres. In this way it can be forced into a tank
above. The rest of the liquid can be run off through the cock, _h_,
at the bottom of the vessel. When quite empty the cover is taken off,
the vessel turned over, and the solid residue removed. One extraction
of dye-woods is not sufficient to remove the whole of the colouring
matter; in most cases the wood is treated a second time before the
apparatus is emptied. Even then some quantity of colouring matter
remains in the wood. The twice extracted wood is brought into a tub
filled with water, and the solution resulting from the long contact
of the water with the wood is used in the next operation to extract
new quantities of wood instead of fresh water. The dimensions of the
extraction vessel vary according to the size of the works. A large
apparatus costs not much more than a smaller, since in both cases the
labour is the same, so that it is advisable to use a large apparatus.
When the copper extraction vessel is made to have its greatest diameter
about 1 metre, it can be charged with about 50 kilogrammes of rasped
wood at once.
[Illustration: FIG. 38.]
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