The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigmentsBersch, Josef
Science
The manufacture of mineral and lake pigments : $b Containing directions for the manufacture of all artificial artists' and painters' colours, enamel colours, soot and metallic pigments
Bersch, Josef
Dyes and dyeing; Pigments
In the preparation of colours liquids have often to be brought into
the precipitating vessel which would attack the iron of the stirring
apparatus, so that it is advisable to make the connecting rods between
the two discs of such a length that the screws may be above the vessel.
All iron parts of the apparatus dipping into the liquid should be
protected by asphaltum varnish.
When a specially heavy precipitate is to be washed, such as enamel
white, chrome yellow or white lead, the stirrer is raised as high
as possible before the commencement of the operation. When the
precipitate has formed and settled, the liquid is run off, the water
tap opened, and the stirrer slowly brought down to the precipitate;
the brushes fastened to the crosspiece stir up first the top of the
precipitate, then the next portions, and so on until the whole of the
precipitate has been stirred up into the liquid. When this has been
accomplished, the stirrer is kept going for some time, so that the
water may take up as much of the soluble materials as possible; it is
then raised out of the vessel, in which the precipitate again settles.
As a rule, two or three washings of permanent white, in an apparatus of
the construction described, are sufficient to render it quite free from
acid. Washing must be continued until the wash water leaves blue litmus
paper quite unchanged. When dry, precipitated barium sulphate is a very
soft powder of great whiteness, which, on account of the fineness of
its particles, can be readily ground with binding materials.
Enamel white loses, in a remarkable manner when completely dry, a great
portion of its covering power and of its valuable property of being
easily ground with oil or size to a homogeneous paste. It is not known
whether this alteration is caused by a molecular change of the barium
sulphate, as is not altogether improbable. In order to preserve the
valuable properties of enamel white it is not, as a rule, completely
dried, but is brought into the market in the form of pulp, which is
obtained by bringing the washed precipitate into strong linen bags
and allowing the water to drop through. This object is more quickly
accomplished when the last wash water is drawn off only to such a point
that, when the precipitate is again mixed up by means of the stirrer,
a thin paste is formed. This paste is run into a centrifugal machine,
of which Fig. 22 is an illustration. In the drum, B, provided with an
outflow, R, the smaller removable drum, C, with perforated walls, is
caused to rotate by gearing, G, to which it is attached by the screw,
V. The drum, C, is lined by a tight linen bag.
[Illustration: FIG. 22.]
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