The Quarterly Journal of Science, Literature and the Arts, July-December, 1827Various
Science
The Quarterly Journal of Science, Literature and the Arts, July-December, 1827
Various
Arts -- Periodicals; Science -- Periodicals; Technology -- Periodicals
23. _Chemical Researches relative to certain Ancient Substances_.—M.
Vauquelin has analyzed, i. A poignard blade formed of copper only;
ii. A mirror, which was found to consist of 85 parts of copper, 14
of tin, and 1 of iron per cent.; iii. A blue colour found in a tomb:
[p210] it was composed of silica 70 parts; lime 9; oxide of copper
15; oxide of iron 1; soda mixed with potash 4. A blue identical with
this, both in colour and composition, was found in the bottom of a
furnace in which copper had been fused at Romilly.
M. D’Arcet has examined a bone from the fore part of an ox, which had
been placed as an offering to the divinity in an Egyptian tomb, and
found that it contained as much gelatine as recent bone, although
rather less is obtained by muriatic acid, (20 per cent. instead of
27) because of a deterioration of the bone. When burnt, it gave an
animal black as deep in colour as that from recent bone.
M. Le Baillif has examined some grains of corn, which were so well
preserved, that when put into boiling water iodine produced the
blue colour dependent upon starch. He also made some experiments on
a gummy substance, and on two cords from a musical instrument; the
latter were of animal substance.
M. Raspail examined some grain which was supposed to be wheat, but
found it to be torrified barley; it was covered with a substance
communicated probably by the oil and incense with which the grains
were bathed when consecrated. Similar grains were obtained by
roasting common barley.
The account of most of these researches is given in the Catalogue
raisonné et historique des Antiquités découvertes en Egypte, by M.
Passalacqua.—_Bull. Univ._ A. vii. 264.
24. _On the Bitter Substance produced by the action of Nitric Acid on
Indigo, Silk, and Aloes_, _by_ M. Just Liebeg.—The process by which
M. Liebeg obtains a pure and uniform substance from the action of
nitric acid on indigo, is as follows:—A portion of the best indigo
is to be broken into small fragments, and moderately heated with
eight or ten times its weight of nitric acid of moderate strength.
It will dissolve, evolving an abundance of nitrous vapours and
swelling up in the vessel. After the scum has fallen, the liquid is
to be boiled, and nitric acid added, whilst any disengagement of red
vapours is occasioned by it. When the liquid has become cold, a large
quantity of semi-transparent yellow crystals will be formed, and if
the operation has been well conducted, no artificial tannin or resin
will be obtained. The crystals are to be washed with cold water, and
then boiled in water sufficient to dissolve them. If any oily drops
of tannin form on the surface of the solution, they must be carefully
removed by touching them with filtering paper. Then filtering the
fluid, and allowing it to cool, yellow brilliant crystalline plates
will be obtained, which will not lose their lustre by washing.
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