The Quarterly Journal of Science, Literature and the Arts, July-December, 1827Various
Science
The Quarterly Journal of Science, Literature and the Arts, July-December, 1827
Various
Arts -- Periodicals; Science -- Periodicals; Technology -- Periodicals
Supposing that this substance might contain a principle analogous to
that latterly observed by M. Pelletier in logwood, &c. a portion of
it was dissolved in strong alcohol, the solution evaporated until
very concentrated, and then poured into cold water, an agglomerated
spongy substance was precipitated, which, after being washed with
cold water and filtered, was triturated with water containing
1/100th of sulphuric acid, and exhibited traces of chemical action
at a temperature of 22° (61°.6 F.) It then deposited a substance
upon the sides of the vessel, and the liquid became yellow and very
acid. The sediment, being carefully washed with water, was of a fine
red colour, varying according to the state of aggregation; it had
no taste or smell; was flexible between the fingers, and was quite
fluid at 55° (131° F.). This substance, which the author has called
_Dracine_, has some analogy with the vegeto-alkalis, although its
affinity for acids is but slight. The sulphate may be obtained, he
says, by adding sulphuric acid diluted with alcohol to an alcoholic
solution of _dracine_, precipitating the mixture by cold water, and
then applying a little heat; the sulphate of dracine collects at the
bottom, is to be washed with cold water until the latter no longer
reddens litmus paper, and then dissolved in hot water. This solution
becomes red by the smallest quantity of alkalis, and may be used as
a very sensible test of their presence. Dracine is also a good test
for acids, assuming a yellow colour with them. The small quantity of
carbonate of lime in filtering paper may be detected by sulphate of
dracine, the yellow solution instantly becoming red from its action,
and thus showing its presence.—_Bull. Univ._ C. xi. p. 157.
37. _Purification of Madder, by the Separation of its Yellow
Colouring Matter_.—The experiments of MM. Kuhlman, Colin, and
Robiquet[36], have induced M. G. H. de Kurrer to publish the means
which he has resorted to for the purification of madder, by the
separation of the yellow colouring matter from it; and thus rendering
it more fit to supply the various red, lilac, violet, and brown
colours which are required upon wool, silk, cotton and linen. Three
tubs or vessels are placed by the side of each other: in summer they
may be in the open air under shelter, but in the winter should be
placed in an airy cellar where the temperature may be retained at 18°
or 20° R. (73° to 77° F.). The first is that in which the soaking and
fermentation is to be effected: it should be 2 feet 8 inches deep,
and 2 feet 6 inches in diameter, for from fifty to fifty-five pounds
of madder. The second, or washing vessel, should be 5-1/2 feet deep,
and 3 feet in diameter; it should have three wooden cocks fixed into
it, the first 2 feet, the second 3 feet, and the third 4 feet from
the bottom. The third tub is for deposition; its height should be
4-1/2 feet, and it should have a cock at 1-1/2 foot from the bottom.
[p220]
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account