The Rare Earths: Their Occurrence, Chemistry, and TechnologyLevy, Stanley Isaac
Science
The Rare Earths: Their Occurrence, Chemistry, and Technology
Levy, Stanley Isaac
Rare earths
~Washing.~--The influence of even small quantities of impurities on the
intensity of the light emitted by a mantle is remarkably great, and the
manufacture requires a degree of care and attention far beyond that
needed in ordinary technical processes. Washing of the fabric in
particular must be very thorough and careful, if a mantle of reasonable
quality is required. If the mineral content of the fabric, _i.e._ the
ash left on incineration, amount to more than 0·03 per cent. of the
total weight, the quality of the mantle is seriously affected.
Particularly is this the case if even the smallest traces of iron come
in contact with the fabric; on this account wooden implements must be
used as far as possible in the washing house, and all iron parts must be
carefully protected so that no water can drip from them on to the
material.
The fabric is used in the form of a long cylindrical tube usually of
about twice the diameter required for the base of the finished mantle.
Before the mineral impurities can be removed, this must be entirely
freed from grease. It is therefore washed thoroughly with a warm
solution of sodium carbonate, which removes all the hydrolysable fats.
If paraffin or other non-hydrolysable grease is present, the alkaline
wash must be followed by a soap wash. The fabric is now cleansed from
alkali and soap by running water, and mineral impurities are removed by
treatment with dilute hydrochloric acid (1-3 per cent.) at a temperature
of 50°-60°C.; it is finally washed free from acid with distilled water.
So susceptible is the mantle to traces of impurity that the use of
ordinary tap water, or even of a distilled water which has become
contaminated to the smallest degree, for this final washing, will
considerably lower its efficiency.
A centrifugal machine removes most of the water, and the drying is
completed by passage over wooden rollers, through a small chamber, of
which the air is kept at 30°-40°C. The dried fabric is now cut into
lengths ready for the next process.
[Illustration: FIG. 11]
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