The Working of Steel: Annealing, Heat Treating and Hardening of Carbon and Alloy SteelColvin, Fred H. (Fred Herbert)
Science
The Working of Steel: Annealing, Heat Treating and Hardening of Carbon and Alloy Steel
Colvin, Fred H. (Fred Herbert)
Steel
If only one instrument, such as a millivoltmeter, is available,
and there is no standard couple at hand, the new couple may be
calibrated over a wide range of temperatures by the use of the following
standards:
Water, boiling point 212 deg.F.
Tin, under charcoal, freezing point 450 deg.F.
Lead, under charcoal, freezing point 621 deg.F.
Zinc, under charcoal, freezing point 786 deg.F.
Sulphur, boiling point 832 deg.F.
Aluminum, under charcoal, freezing point 1,216 deg.F.
Sodium chloride (salt), freezing point 1,474 deg.F.
Potassium sulphate, freezing point 1,958 deg.F.
A good practice is to make one pyrometer a standard; calibrate it
frequently by the melting-point-of-salt method, and each morning
check up every pyrometer in the works with the standard, making the
necessary corrections to be used for the day's work. By pursuing
this course systematically, the improved quality of the product
will much more than compensate for the extra work.
The purity of the substance affects its freezing or melting point.
The melting point of common salt is given in one widely used handbook
at 1,421 deg.F., although chemically pure sodium chloride melts at
1,474 deg.F. as shown above. A sufficient quantity for an extended
period should be secured. Test the melting point with a pyrometer
of known accuracy. Knowing this temperature it will be easy to
calibrate other pyrometers.
PLACING OF PYROMETERS.--When installing a pyrometer, care should be
taken that it reaches directly to the point desired to be measured,
that the cold junction is kept cold, and that the wires leading to
the recording instrument are kept in good shape. The length of
these lead wires have an effect; the longer they are, the lower
the apparent temperature.
When pyrometers placed in a number of furnaces are connected up
in series, and a multiple switch is used for control, it becomes
apparent that pyrometers could not be interchanged between furnaces
near and far from the instrument without affecting the uniformity
of product from each furnace.
Calibration can best be done without disturbing the working pyrometer,
by inserting the master instrument into each furnace separately, place
it alongside the hot junction of the working pyrometer, and compare
the reading given on the indicator connected with the multiple
switch.
Protection tubes should be replaced when cracked, as it is important
that no foreign substance is allowed to freeze in the tube, so
that the enclosed junction becomes a part of a solid mass joined
in electrical contact with the outside protecting tube. Wires over
the furnaces must be carefully inspected from time to time, as no
true reading can be had on an instrument, if insulation is burned
off and short circuits result.
If the standard calibrating instrument used contains a dry battery,
it should be examined from time to time to be sure it is in good
condition.
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