The works of the highly experienced and famous chymist, John Rudolph Glauber : $b containing, great variety of choice secrets in medicine and alchymy in the working of metallick mines, and the separation of metals: also, various cheap and easie ways of making salt-petre, and improving of barren-land, and the fruits of the earth.Glauber, Johann Rudolf
Science
The works of the highly experienced and famous chymist, John Rudolph Glauber : $b containing, great variety of choice secrets in medicine and alchymy in the working of metallick mines, and the separation of metals: also, various cheap and easie ways of making salt-petre, and improving of barren-land, and the fruits of the earth.
Glauber, Johann Rudolf
Alchemy -- Early works to 1800; Chemistry -- Early works to 1800; Medicine, Magic, mystic, and spagiric -- Early works to 1800
In the same manner as was taught of Zinck, there may be out of lead
also distilled a subtle spirit and a sweet oyl, and it is done thus:
Pour strong vinegar upon _Minium_, or any other calx of lead, which
is made _per se_, and not with sulphur, let it digest and dissolve in
sand or warm ashes, so long till the vinegar be coloured yellow by the
lead, and turned quite sweet. Then pour off the clear solution, and
pour on other vinegar, and let this likewise dissolve, and this repeat
so often, till the vinegar will dissolve no more, nor grow sweet;
then take all these solutions, and evaporate all the moisture, and
there will remain a thick sweet yellow liquor, like unto honey, if the
vinegar was not distilled, but if it was distilled and made clear, then
no liquor remaineth, but only a white sweet salt. This liquor or salt
may be distilled after the same manner as was taught with the Zinck,
and there will come over not only a penetrating subtle spirit, but also
a yellow oyl, which will not be much, but very effectual, in all the
same uses, as of the spirit, and oyl of the Zinck was taught.
N. B. This is to be observed, that for to make this spirit and oyl,
you need no distilled spirit, but that it may be done as well with
undistilled vinegar, and the undistilled yields more spirit than the
distilled. But if you look for a white and clear salt, then the vineger
must be distilled, else it doth not shoot into crystals, but remaineth
a yellow liquor like unto honey, and it is also needless to make the
solution in glasses, and by digestion continued for a long time, but it
may as well be done in a glazed pot, _viz._ pouring the vinegar upon
the Mineum in the pot, and boyling it on a coal fire; for you need not
fear that any thing of the vinegar will evaporate, in regard that the
lead keeps all the spirits, and lets only go an unsavory phlegm. You
must also continually stir the lead about with a wooden spatulla, else
it would turn to a hard stone, and would not dissolve: the same must
be done also when the solution is done in glasses; and the solution
after this way may be done in three or four hours: and when both kind
of solutions are done, there will be no difference betwixt them, and I
think it providently done not to spend a whole day about that which may
be done in an hour.
And if you will have this spirit and oyl better and more effectual, you
may mix ℥ i. of crude Tartar made into powder with ℔ j. of dissolved
and purified lead, and so distil it after the same manner as you do
distil it by it self, and you will get a much subtler spirit and a
better oyl than if it were made alone by it self.
_To distil a subtile spirit and oyl out of crude Tartar._
Public-domain text, read in full here on John Shaqi.
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