The works of the highly experienced and famous chymist, John Rudolph Glauber : $b containing, great variety of choice secrets in medicine and alchymy in the working of metallick mines, and the separation of metals: also, various cheap and easie ways of making salt-petre, and improving of barren-land, and the fruits of the earth.Glauber, Johann Rudolf
Science
The works of the highly experienced and famous chymist, John Rudolph Glauber : $b containing, great variety of choice secrets in medicine and alchymy in the working of metallick mines, and the separation of metals: also, various cheap and easie ways of making salt-petre, and improving of barren-land, and the fruits of the earth.
Glauber, Johann Rudolf
Alchemy -- Early works to 1800; Chemistry -- Early works to 1800; Medicine, Magic, mystic, and spagiric -- Early works to 1800
_The way or manner to perform the Distillation._
When you intend to distil, then first make a fire in the Furnace, that
the distilling vessel come to be very hot. But if it be not fastned
to the Furnace, then set it upon a grate, and lay stones about it,
and coals between, and so let it grow hot, and lay melted lead in the
space between the two edges or brims, to the end, that the lid, when it
is put on, may close exactly, so that no spirit can get through. This
done, take a little of the matter you intend to distil, and cast it in,
and presently put on the lid, and there will be no other passage left
but through the pipe, to which there must be applyed and luted a very
big receiver. As soon as the species cast in come to be warm, they let
go their spirit, which doth come forth into the receiver: and because
there was but little of the matter cast in, it hath no power to force
through the lute, or to break the receiver, but must settle it self.
This done, cast in a little more of your matter, cover it and let it go
till the spirit be settled: continue this proceeding so long, until you
have spirits enough: but take heed, that you cast in no more at once,
than the receiver is able to bear, else it will break. And when your
vessel is full, the distillation not being ended, then take off the
lid, and with an iron ladle take out the Caput Mortuum; and so begin
again to cast in, and still but a little at a time, and continue this
as long as you please.
Thus in one day you may distil more in a small vessel, than otherways
you could do in a great retort; and you need not fear the least loss of
the subtile spirit, nor the breaking of the receiver by the abundance
of the spirits: and you may cease or leave off your distilling, and
begin it again when you list: also the fire cannot be made too strong,
so that it might cause any hurt or damage; but by this way you may
make the most subtile spirits, which is impossible to be done by any
Retort. But if you will distil a subtil spirit by a Retort, as of
Tartar, Harts-horn, Salarmoniack, or the like, you cannot do it without
prejudice (though there were but half a pound of the matter in it) the
subtlest spirits coming forth with force, seek to penetrate through
the lute, if that be not good, but if that be good, so that the spirits
cannot pass through it, then they break the receiver, because it cannot
possibly hold such a quantity of subtle spirits at once. For when they
are coming, they come so plentifully, and with such a force, that the
receiver cannot contain them, and so of necessity must flye asunder,
or must pass through the lutum; All which is not to be feared here,
because there is but a little cast in at once, which cannot yield such
a quantity of spirits, as to force the receiver to break: And when
there comes forth no more spirits, and the former is settled, then more
of the matter is to be cast in; and this is to be continued so long,
until you have spirits enough.
Public-domain text, read in full here on John Shaqi.
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