A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
The principle of compound distillation is well shown in Dorn's apparatus,
Fig. 12. This consists of a still or boiler _A_ having a large
dome-shaped head, on the interior faces of which the alcoholic vapors
will condense. Thus only enriched vapors will pass up through goose-neck
_B_ to the mash heater _D_. _C_ is a worm the end of which passes out to
a compartment _E_ through an inclined partition _F_. From the compartment
_E_ a pipe _e_ leads into the still _A_. An agitator _H_ is used for
stirring the mash, so that it may be uniformly heated. A pipe _d_
provided with a cock allows the mash to be drawn off into the still _A_.
From the highest point of the compartment _E_ a pipe _M_ leads to
condensing coil _K_ in a tub _J_ of cold water, having a draw-off cock
_I_.
At the exit end of the condensing worm _K_ the tube is bent in a U form
as at _L_, one arm of which has a curved open-ended continuation _n_,
through which the air in the worm is expelled. The other arm opens into
an inverted jar _l_ containing a hydrometer, for indicating the strength
of the spirit. The spirits pass off through _m_ into a receiver.
In operation the mash is admitted into the heater _D_ through _G_ until
the heating tank is nearly filled. A certain amount of mash is then
allowed to run into the still _A_ through the pipe _d_. The cock in _d_
is closed and the fire lighted.
The vapors from the still are condensed in worm _C_ and the condensed
liquid drops down into compartment _E_. Any vapor passing through _B_ and
_C_ so highly heated as to be uncondensed in coils _C_ passes through
the layer of liquid in compartment _E_, collects in the highest portion
of the compartment and passes through pipe _M_ to coil _K_ where it is
entirely liquefied. If the liquid in _E_ rises beyond a certain level it
passes through pipe _e_ back to the still. Any vapors which may collect
in the upper part of _D_ pass into the small bent pipe opening into the
first coil of worm _C_. Water for rinsing the heater _D_ may be drawn
through cock _s_ from the tub _J_ and warm water for rinsing the still,
through pipe _d_ from the heater.
Another form of compound still is shown in Fig. 13. In this the still _S_
is divided into an upper and lower compartment by a concavo-convex
partition _d_, having at its crown an upwardly extending tube _t_ from
which projects side tubes _p_. A pipe _P_ opens above and extends from
tube _t_. _C_ is the mash heater and condenser. Connected to the head of
the still is a pipe _T_ through which the vapors pass to a condensing
coil _f_ formed on the wall of the heater _C_. At its bottom the coil _f_
extends out of the heater, through the water tub _W_ and out to receiver
as at _F_. In the heat of this heater is a valve _V_ whereby any vapors
which may arise from the heated mash are conducted by pipe _U_ to _T_.
Public-domain text, read in full here on John Shaqi.
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