A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
In its course downwards the wash is met by the steam passing up through
the perforations, and the whole of the spirit which it contains is thus
converted into vapor. As soon as the chamber _B_ is nearly full of the
spent wash, its contents are run off into the lower compartment by
opening a valve in the pipe _V_. By means of the cock _E_, they are
finally discharged from the apparatus. This process is continued until
all the wash has been pumped through.
The course taken by the steam will be readily understood by a glance at
the figure. When it has passed through each of the chambers of the
analyzer, the mixed vapors of water and spirit pass through the pipe _i_
into the rectifying column. Ascending again, they heat the coiled pipe
_m_, and are partially deprived of aqueous vapors by condensation. Being
thus gradually concentrated, by the time they reach the opening at _w_
they consist of nearly pure spirit, and are then condensed by the cool
liquid in the pipe, fall upon the partition and are carried away by the
pipe _y_ to a refrigerator _W_. Any uncondensed gases pass out by the
pipe _R_ to the same refrigerator, where they are deprived of any alcohol
they may contain. The weak liquor condensed in the different compartments
of the rectifier descends in the same manner as the wash descends in the
other column; as it always contains a little spirit, it is conveyed by
means of the pipe _S_ to the vessel _L_ in order to be pumped once more
through the apparatus.
=The condensed spirit= gathered over the plates _v_ passes out through
the pipe _y_ to the condensing worm _T_. If any vapors escape the
condensing plates they pass into _R_ and are condensed in the worm _T_
also. From worm _T_ the spirit flows into a suitable receiver _Z_.
Before the process of distillation commences, it is usual, especially
when the common Scotch stills are employed, to add about one lb. of soap
to the contents of the still for every 100 gallons of wash. This is done
in order to prevent the liquid from boiling over, which object is
effected in the following way: The fermented wash always contains small
quantities of acetic acid; this acts upon the soap, liberating an oily
compound which floats upon the surface. The bubbles of gas as they rise
from the body of the liquid are broken by this layer of oil, and hence
the violence of the ebullition is considerably checked. Butter is
sometimes employed for the same purpose.
Figs. 19 and 20 show a diagrammatic section and a plan of a still used
for thick mashes which are liable to burn. This comprises a circular
chamber _B_ supported over suitable heating means, having on its bottom a
series of concentric partitions _b_ which divide the bottom of the
chamber into shallow channels for the mash. Running diametrically through
the chamber is a partition.
[Illustration: FIG. 19.--Rotary Current Still.]
Public-domain text, read in full here on John Shaqi.
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