A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
The rich and highly vaporized vapors which have passed the test of this
preliminary concentration, pass out of the compartment _f_ by a pipe _M_.
Here again the water surrounding the pipe tends to condense all but the
most highly charged vapor and send it back to compartment _f_ but the
vapor which succeeds in passing over through pipe _G_ is carried downward
to a condenser _H_ where it is finally condensed and drawn off as at _g_.
It is necessary that the rate of mash feed be regulated so that neither
too much mash shall be pumped into the mash heater _G_, or too little,
and the pipe leading from the pump to the heater is therefore provided
with a tap and an indicating dial.
In these modern stills the following are particularly important points to
be especially brought to the consideration of the distiller.
It cannot be too strongly impressed that effectiveness of the distilling
column depends on the plates dividing it,--that is, upon the
horizontality of the plates and the form of the traps or perforations. If
the plates are not horizontal the wash is not maintained at a uniform
level across the entire extent of the plate and hence some of the
ascending vapor will pass out without contacting with the wash through
uncovered traps, while others of the traps will be so deeply submerged in
wash that the vapor cannot bubble through.
Again the caps should be so made as to divide the vapor into fine streams
and bring it into contact with each part of the wash. Plates simply
perforated and uncapped give excellent results for they molecularize the
vapor ascending through the liquid contained on the plates, but they
require a constant pressure of vapor, and any variations of pressure
tends to discharge them. In addition these perforations gradually enlarge
by the action of acids in the wash or clog up, and the apparatus soon
works badly.
Good forms of capped traps are those shown in Figs. 24, 25 devised by
Barbet. These are provided with an interior upwardly projecting rim.
Extending over the rim and down around it is a copper cap having its
margin slitted.
The wash carried on the plate circulates about the caps and the alcoholic
vapors bubble out through the slits and up through the wash, the vapor
thus being finely divided and coming into intimate contact with each
portion of the wash and thus more thoroughly depriving it of its alcohol.
[Illustration: FIG. 24.--Barbet Trap.]
[Illustration: FIG. 25.--Barbet Trap.]
Besides this there is another advantage resident in these caps, namely,
that distillation may be stopped for several hours and then re-started
without trouble for the reason that the wash has been retained on the
plates, whereas were the plates simply perforated the wash would ooze
through and the plates have to be recharged. This form of plate may be
easily repaired and does not necessitate the removal or replacement of
the plate itself. The caps alone need be removed.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account