A Practical Handbook on the Distillation of Alcohol from Farm Products — John Shaqi
A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
Fig. 38 represents a simple rectifying apparatus designed for small or
medium sized plants, and manufactured by the Vulcan Copper Works Co., of
Cincinnati. The still is upright, with a chambered column above it, of
the usual type. The chambers are fitted with a vapor boiling pipe and cap
and a drop pipe, and each is provided with cocks whereby it may be
drained for cleansing. Above the column is a separator, comprising a
casing containing a series of tubes. The vapor from the column circulates
around the tubes through which passes a current of cool water. The
condenser is of the same construction as the separator and is provided
with a gage glass and a draw-off cock. The operation is the same as in
other simple rectifiers; part of the vapor from the column is condensed
in the separator and passes back on to the upper plates, while the more
highly vaporized portions pass over into the condenser.
[Illustration: FIG. 38.--Rectifying Apparatus with External Tubular
Condenser. (_To face page 94_)]
The diameter of the still is large relatively to its depth so as to yield
an economical and at the same time highly effective distribution of heat
through the charge. This also affords an extended boiling area from which
the vapor rises evenly and regularly, thus ensuring conditions peculiarly
conducive to produce the best fractionating. The floor space required for
this still and others of the same character built by this company is very
compact and excessive weight on the top floor of the building is
dispensed with.
We have shown in Figs. 39 and 40 two forms of rectifying apparatus, one a
twin column Barbet rectifier and the other a rectifier of the Gillaume
type combined with inclined column still.
[Illustration: FIG. 39.--Twin Column Barbet Rectifier.]
In the twin column apparatus, Fig. 39, the first column or clarifier _A_
receives the raw phlegm and accomplishes the elimination of ethers. The
clarified phlegm passes then to the second column where the alcohol
is separated from the last runnings or fusel oil. In other words, the
phlegm or impure raw alcohol is only raised to such a temperature in the
first column as to drive off the very volatile constituents such as the
ethers. These therefore pass off at the top of the first column into the
condenser _C_, the retrogradation or condensed alcohol being returned to
_A_, while the boiling phlegm taken from the middle of the column and
still containing the aldehydes, oils, etc., is conducted by a pipe _E_ to
the second column _B_ wherein the last runnings or amylic oils, etc., are
separated from the purified spirits.
The vapors in this column are carried to the condensers _D_ and _F_ and
from there to a refrigerator _G_. The fusel oils are extracted from the
plates slightly below the center of the column and are carried to an oil
concentrating apparatus _H_.
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