A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
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A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
Lately a combination of the écuelle and distilling processes has been
introduced by Domenico Monfalcone, which has given excellent results.
It is shown in Fig. 20. _F F_ is a hollow cylinder, of sheet-iron,
the interior surface of which is studded with a large number of
small metallic knife-points. This cylinder revolves on two axles
attached to it at diagonally opposite points. The cylinder having been
half-charged with lemons, together with a small quantity of water, is
set in motion by aid of the shafting and pulleys driven by the small
steam engine. The fruits are thereby made to come in contact with the
metallic lancets, and their whole surface gradually becomes punctured
sufficiently to rupture the cells containing the volatile oil, which
escapes. The cylinder _F F_ has double walls, the space between them
being intended for the circulation of a current of steam, which is
admitted to heat the water and to facilitate the extraction of the
oil, while at the same time the vapors are rarefied or aspirated by
the vacuum pump _L_. The axles of the cylinder on both sides are
hollow; that on the side looking towards the engine is imbedded in
such a manner that steam from the boiler _D_ may be admitted at will,
either into the double walls of the cylinder, or into the interior
of the cylinder itself, while the hollow passage in the other axle
communicates with a condensing worm, _G_, the outlet of which, _H_,
descends into a cylindrical vessel, _I_, intended to receive the
condensed products, consisting of water and volatile oil. When the
apparatus is first set in motion the pump _L_ begins to produce a
vacuum during the first revolutions of the cylinder. Steam being now
cautiously admitted into the double walls of the cylinder, the water is
raised to boiling at a comparatively low temperature, and the vapors
charged with the volatile oil pass over into the receptacle, where
they separate into two layers. The product obtained by this process is
claimed to be equal in quality to that obtained by mechanical means,
and the yield nearly double.
During the months of November to March the average yield from 1000
lemons in the factories of Palermo is 320 grammes of oil; in those of
Messina, where a better quality of fruit is employed, the yield is
about 400 grammes. The same number of lemons yield about 10 gallons of
juice, the collection of which is, of course, a necessary accompaniment
of the manufacture of volatile oil.
Pure oil of lemons is almost colorless and has the odor of the fruit.
Its specific gravity varies between 0.8752 and 0.8785; it boils at
298.4° F., and is soluble in all proportions in absolute alcohol and
glacial acetic acid. It contains, according to G. Bouchardat and
J. Lafont, besides a little cymene, several hydrocarbons, the most
abundant of which is citrene, C_{10}H_{16}, boiling near 352.5° F.,
having a rotatory power exceeding +105°, and yielding a solid optically
inactive dihydrochloride.
Public-domain text, read in full here on John Shaqi.
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