A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
To produce an efficient flame of oxidation, put the point of the
blowpipe into the flame about one third the diameter of the wick, and
about one twelfth of an inch above it. This, however, depends upon
the size of the flame used. Blow strong enough to keep the flame
straight and horizontal, using the largest orifice for the purpose.
Upon examining the flame thus produced, we will observe a long, blue
flame, _a b_, Fig. 3, which letters correspond with the same letters
in Fig. 2. But this flame has changed its form, and contains all the
combustible gases. It forms now a thin, blue cone, which converges to
a point about an inch from the wick. This point of the flame possesses
the highest intensity of temperature, for there the combustion of the
gases is the most complete. In the original flame, the hottest part
forms the external envelope, but here it is compressed more into a
point, forming the cone of the blue flame, and likewise an envelope of
flame surrounding the blue one, extending beyond it from _a_ to _c_,
and presenting a light bluish or brownish color. The external flame
has the highest temperature at _d_, but this decreases from _d_ to
_c_.
[Illustration: Fig. 3]
If there is a very high temperature, the oxidation is not effected so
readily in many cases, unless the substance is removed a little from
the flame; but if the heat be not too high, it is readily oxidized in
the flame, or near its cone. If the current of air is blown too
freely or violently into the flame, more air is forced there than is
sufficient to consume the gases. This superfluous air only acts
detrimentally, by cooling the flame.
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