A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
These metals are infusible before the blowpipe. They are not volatile,
nor are they oxidizable. Their oxides are, in both flames, reduced to
a metallic and infusible powder. They give no reactions with fluxes,
but are separated in the metallic form. These metals are generally
found associated together in the native platinum, also with traces of
copper, lead, and iron.
The metal palladium is found native, associated with iridium and
platinum. This metal generally occurs in greatest quantity in Brazil.
The metal rhodium is found along with platinum, but in very small
quantities.
Iridium occurs in nature associated with osmium, gold, and platinum,
in the mines of Russia. Its great hardness has rendered it desirable
for the points of gold pens. In South America this metal is found
native, associated with platinum and osmium. The latter metal,
associated with platinum and iridium, has been found in South America.
As these metals will not oxidize or dissolve, they cannot be separated
from each other by the blowpipe with the reagents peculiar to that
species of analysis. It is true that colors may be discerned in the
beads, but these tints proceed from the presence of small traces of
copper, iron, etc.
The ore of osmium and iridium can be decomposed, and the former
recognized by its fetid odor. This metal, strongly ignited in a glass
tube with nitrate of potash, is converted to the oxide of osmium,
which gives an odor not unlike the chloride of sulphur.
As the metals of this group are very rare ones, especially the last
four ones, we shall not devote an especial division to each of them.
For a more detailed statement of their reactions, the student is
referred to the large works upon blowpipe analysis.
CLASS III.
NON-METALLIC SUBSTANCES.
1. _Water_--2. _Nitric Acid_--3. _Carbon_--4. _Phosphorus_
--5. _Sulphur_--6. _Boron_--7. _Silicon_--8. _Chlorine_
--9. _Bromine_--10. _Iodine_--11. _Fluorine_--12. _Cyanogen_
--13. _Selenium_.
(1.) _Water_ (HO).--Pure distilled water is composed of one volume of
oxygen, and two volumes of hydrogen gases; or, by weight, of one part
of hydrogen to eight parts of oxygen gases. Water is never found pure
in nature, but possessing great solvent properties, it always is found
with variable proportions of those substances it is most liable to
meet with, dissolved in it. Thus it derives various designations
depending upon the nature of the substance it may hold in solution, as
lime-water, etc.
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