A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
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A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
Formula. [.Fe]^{3}[.....As] +
[...Fe=]^{3}[.....As]^{2} + 18[.H].
Behavior
(1) in glass-bulb. Evolves much water.
(2) in open tube. As the preceding.
(3) on charcoal. As the preceding.
(4) in forceps. As the preceding.
(5) in borax. As the preceding.
(6) in mic. salt. As in borax.
(7) with carb. soda. As the preceding.
(8) Special reactions. As the preceding.
* * * * *
MANGANESE.
* * * * *
Mineral. Manganblende
Formula. MnS.
Behavior
(1) in glass-bulb. --
(2) in open tube. Gives off SO^{2} and becomes greyish green on
surface.
(3) on charcoal. Is slowly roasted and converted into oxide.
(4) in forceps. V.
(5) in borax. The roasted mineral gives a strong manganese
reaction.
(6) in mic. salt. In the unroasted state, dissolves with much
ebullition and detonation due to elimination of
sulphide of phosphorus. The bead then exhibits
the characteristic violet color of manganese.
(7) with carb. soda. Forms a slaggy mass, which laid on silver and
moistened, gives the sulphur reaction.
(8) Special reactions. --
* * * * *
Mineral. Pyrolusite
Formula. [..Mn].
Behavior
(1) in glass-bulb. Frequently gives off a small quantity of water
and, when strongly heated, oxygen.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V.
(5) in borax. Gives the manganese reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. Forms a slaggy mass.
(8) Special reactions. --
* * * * *
Mineral. Manganite
Formula. [...Mn=][.H].
Behavior
(1) in glass-bulb. Gives off much water.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V. Exfoliates slightly.
(5) in borax. As the preceding.
(6) in mic. salt. As in borax.
(7) with carb. soda. As the preceding.
(8) Special reactions. --
* * * * *
Mineral. Psilomelane
Formula. ([.Ba],[.Ca],[.Mg],[.K]) [..Mn] + [.H].
Behavior
(1) in glass-bulb. Gives off water and, when
strongly heated, oxygen.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V. Colors flame faintly green(Ba) and red
towards the point (Ca).
(5) in borax. As pyrolusite.
(6) in mic. salt. As in borax.
(7) with carb. soda. As pyrolusite.
(8) Special reactions. --
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