A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
* * * * *
Mineral. Wad
Formula. [..Mn],[.Mn],[.H], also [...Fe=],[...Al=],
[.Ba],[.Cu],[...Pb],[...Si], etc.
Behavior
(1) in glass-bulb. Gives off water.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V. Colors flame variously according to its
composition.
(5) in borax. Gives the manganese reaction, more or less
modified by the presence of other oxides.
(6) in mic. salt. As in borax.
(7) with carb. soda. As pyrolusite.
(8) Special reactions. Various according to composition. When strongly
heated and then moistened has an alkaline
reaction on red litmus paper.
* * * * *
Mineral. Rhodonite
Formula. [.Mn]^{3}[...Si]^{2}.
Behavior
(1) in glass-bulb. Gives off more or less water.
(2) in open tube. --
(3) on charcoal. Under a strong flame fuses to a brown opaque
bead.
(4) in forceps. II. As on charcoal.
(5) in borax. In the oxidizing flame gives the manganese
reaction. In reducing flame the iron reaction.
(6) in mic. salt. As in borax, but leaves an insoluble siliceous
skeleton.
(7) with carb. soda. With a small quantity of the alkali fuses to a
black bead. With a larger quantity forms a slag.
(8) Special reactions. --
* * * * *
Mineral. Diallogite
Formula. [.Mn][..C].
Behavior
(1) in glass-bulb. Frequently decrepitates and gives off more or
less water.
(2) in open tube. --
(3) on charcoal. If strongly heated and moistened has an alkaline
reaction on litmus paper due to the presence of
Ca.
(4) in forceps. V. Frequently colors the flame slightly red.
(5) in borax. Gives the manganese and iron reactions.
(6) in mic. salt. As in borax.
(7) with carb. soda. Forms an infusible slag.
(8) Special reactions. In warm acid dissolves with much effervescence.
* * * * *
Mineral. Triplite
Formula. ([..Mn][.Fe])^{4}[.....P].
Behavior
(1) in glass-bulb. Generally gives off more or less
water.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. I. Colors the outer blowpipe flame green
([.....P]).
(5) in borax. Gives the manganese and iron reactions.
(6) in mic. salt. As in borax.
(7) with carb. soda. Forms an infusible mass.
(8) Special reactions. --
* * * * *
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