A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
Formula. Cu.
Behavior
(1) in glass-bulb. --
(2) in open tube. --
(3) on charcoal. Fuses to a brilliant metallic bead, which on
cooling becomes covered with a coating of black
oxide.
(4) in forceps. Fuses and colors the outer flame blue.
(5) in borax. In the oxidizing flame dissolves and then gives
the copper reactions.
(6) in mic. salt. As in borax.
(7) with carb. soda. --
(8) Special reactions. --
* * * * *
Mineral. Vitreous Copper
Formula. Cu^{2}S.
Behavior
(1) in glass-bulb. --
(2) in open tube. Evolves SO^{2} and, when pulverized and gently
heated for some time is converted into CuO.
(3) on charcoal. Fuses to a bead, which spirts considerably and
gives off SO^{2}. When pulverized and gently
roasted, is converted into CuO.
(4) in forceps. --
(5) in borax. The roasted mineral gives the copper reaction,
and sometimes also a slight iron-reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. In the reducing flame is decomposed, forming NaS
and metallic copper. If the former be cut out
and laid upon silver, it gives the sulfur
reaction.
(8) Special reactions. --
* * * * *
Mineral. Copper pyrites
Formula. [,Cu=][,,,Fe=].
Behavior
(1) in glass-bulb. Decrepitates, sometimes gives a sublimate of
sulphur and becomes bronze colored on the
surface.
(2) in open tube. Evolves SO^{2} and is finally converted into a
dark red mixture of Fe^{2}O^{3} and CuO.
(3) on charcoal. Fuses readily with much ebullition and is
magnetic on cooling.
(4) in forceps. --
(5) in borax. As the preceding; but when the copper has been
removed by reducing on charcoal, the bead shows
a strong iron color.
(6) in mic. salt. As the preceding, but the color in the oxidizing
flame is green, owing to the presence of iron.
(7) with carb. soda. Yields a bead of metallic copper and some
magnetic oxide of iron which remains on the
charcoal. The fused gives a sulphur reaction on
silver.
(8) Special reactions. --
* * * * *
Mineral. Fahlerz
Formula. ([,Cu=][,Ag][,Fe][,Zn])^{4} ([,,,Sb][,,,As]).
Behavior
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