A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
(2) in open tube. Evolves thick white fumes of [...Sb],[.....Sb]
and [.Pb][...Sb]. Also [.S].
(3) on charcoal. Fuses readily and incrusts the charcoal with
[...Sb] and [.Pb] leaving a dark colored bead.
(4) in forceps. --
(5) in borax. If the bead obtained on charcoal be fused on
that support in the reducing flame with borax, a
slight iron reaction is obtained, and after a
time a copper reaction.
(6) in mic. salt. As with borax.
(7) with carb. soda. Yields a bead of metallic copper and lead and
incrusts the charcoal with [...Sb] and [.Pb].
The alkaline mass laid on silver and moistened
gives the sulphur reaction.
(8) Special reactions. --
* * * * *
Mineral. Red oxide of copper
Formula. Cu^{2}O
Behavior
(1) in glass-bulb. --
(2) in open tube. Is converted into the black oxide CuO.
(3) on charcoal. In the reducing flame is reduced, forming a
bead of metallic copper.
(4) in forceps. Fuses and colors the the flame emerald
green, or if previously moistened with HCl,
blue.
(5) in borax. Gives the copper reaction.
(6) in mic. salt. As with borax.
(7) with carb. soda. Is reduced to a bead of metallic copper.
(8) Special reactions. --
* * * * *
Mineral. Atacamite
Formula. CuCl + 3[.Cu] + 6[.H].
Behavior
(1) in glass-bulb. Gives off much water, having an acid
reaction, on test paper, and forms a light
grey sublimate of CuCl.
(2) in open tube. --
(3) on charcoal. Fuses, colors the flame blue, forms a brown
and a pale grey incrustation on the
charcoal, and is reduced to metallic copper,
leaving a small quantity of slag.
(4) in forceps. Fuses and colors the outer flame intensely
blue and green towards the point.
(5) in borax. Gives the copper reactions.
(6) in mic. salt. As with borax.
(7) with carb. soda. Is reduced, yielding a bead of metallic
copper.
(8) Special reactions. --
* * * * *
Mineral. Dioptase
Formula. [.Cu]^{3}[...Si]^{2} + 3[.H].
Behavior
(1) in glass-bulb. Gives off water and turns black.
(2) in open tube. --
(3) on charcoal. In the oxidizing flame becomes black. In the
reducing flame red.
(4) in forceps. V. Colors the outer flame intensely green.
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