A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
(2) in open tube. Fuses and gives off SO^{2}, which passes off
up the tube, and dense white fumes of
SbO^{3} and SbO^{5} which are partly
deposited in the tube.
(3) on charcoal. Fuses and is partly absorbed by the charcoal
and partly volatilized, incrusting the
charcoal with the characteristic white
oxides. Colors the flame blue.
(4) in forceps. --
(5) in borax. As the preceding.
(6) in mic. salt. As in borax.
(7) with carb. soda. Fuses and is reduced, yielding metallic
antimony, which behaves as the preceding
mineral upon charcoal. The alkaline mass
gives the sulphur reaction.
(8) Special reactions. As the preceding.
* * * * *
Mineral. Antimony blende
Formula. [,,,Sb]^{2} + [...Sb].
Behavior
(1) in glass-bulb. Fuses easily, gives off first SbO^{3} and
afterwards an orange colored sublimate.
Strongly heated, is decomposed and gives a
black sublimate, which becomes brown on
cooling.
(2) in open tube. As the preceding.
(3) on charcoal. As the preceding.
(4) in forceps. --
(5) in borax. As native antimony.
(6) in mic. salt. As in borax.
(7) with carb. soda. As the preceding.
(8) Special reactions. As native antimony.
* * * * *
Mineral. White antimony
Formula. SbO^{3}.
Behavior
(1) in glass-bulb. Is sublimed and recondensed in the neck of
the tube.
(2) in open tube. As in the glass-bulb.
(3) on charcoal. Fuses with the evolution of dense white
fumes, which incrust the surface of the
charcoal. In the reducing flame is partly
reduced, yielding metallic antimony. Colors
flame blue.
(4) in forceps. Fuses and is volatilized, coloring the outer
flame blue.
(5) in borax. Gives the antimony reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. In the reducing flame is reduced, yielding
metallic antimony.
(8) Special reactions. As native antimony.
* * * * *
ARSENIC.
* * * * *
Mineral. Native arsenic
Formula. As.
Behavior
(1) in glass-bulb. Sublimes without fusion and recondenses as a
dark grey metallic sublimate, sometimes
leaving a small residue.
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