A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
(2) in open tube. If gently heated in a good current of air
passes off as AsO^{3}, which is partly
condensed as a white sublimate in the upper
part of the tube.
(3) on charcoal. Passes off as AsO^{3}, which thinly incrusts
the charcoal beyond the assay.
(4) in forceps. Colors the flame blue.
(5) in borax. --
(6) in mic. salt. --
(7) with carb. soda. --
(8) Special reactions. --
* * * * *
Mineral. Realgar
Formula. AsS^{2}.
Behavior
(1) in glass-bulb. Fuses, enters into ebullition and is
sublimed as a transparent red sublimate.
(2) in open tube. Gently heated passes off as SO^{2} and
AsO^{3}, the latter of which is redeposited
in the upper part of the tube.
(3) on charcoal. Fuses and passes off as arsenious and
sulphurous acids.
(4) in forceps. Fuses and colors the flame blue.
(5) in borax. --
(6) in mic. salt. --
(7) with carb. soda. As on charcoal, except that the S combines
with the alkali forming NaS, which on silver
gives the sulphur reaction.
(8) Special reactions. --
* * * * *
Mineral. Orpiment
Formula. AsS^{3}.
Behavior
(1) in glass-bulb. As the preceding, except that the sublimate
is of a dark yellow color when cold.
(2) in open tube. As the preceding.
(3) on charcoal. As the preceding.
(4) in forceps. As the preceding.
(5) in borax. --
(6) in mic. salt. --
(7) with carb. soda. As the preceding.
(8) Special reactions. --
* * * * *
Mineral. White arsenic
Formula. AsO^{3}.
Behavior
(1) in glass-bulb. Sublimes without fusion and re-condenses in
white crystals.
(2) in open tube. --
(3) on charcoal. Sublimes and is partly recondensed on
charcoal forming a white incrustation.
(4) in forceps. Colors the flame blue.
(5) in borax. --
(6) in mic. salt. --
(7) with carb. soda. --
(8) Special reactions. Heated with charcoal in a glass-tube sealed
at one end, is reduced and metallic arsenic
sublimes.
* * * * *
MERCURY.
* * * * *
Mineral. Native mercury
Formula. Hg.
Behavior
(1) in glass-bulb. Volatilizes with little or no residue and
recondenses in neck of bulb.
(2) in open tube. --
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account