A system of pyrotechny : $b Comprehending the theory and practice, with the application of chemistry; designed for exhibition and for war.Cutbush, James
History
A system of pyrotechny : $b Comprehending the theory and practice, with the application of chemistry; designed for exhibition and for war.
Cutbush, James
Fireworks; Military fireworks
Mr. James (_Military Dictionary_, p. 348) says, that it has been
recommended to preserve gunpowder at sea by means of boxes lined with
sheet-lead. M. D. Gentien, a naval officer, tried the experiment by
lodging a quantity of gunpowder and parchment cartridges in a quarter
of the ship which was sheathed in this manner. After they had been
stowed for a considerable time, the gunpowder and cartridges were
found to have suffered little from the moisture; whilst the same
quantity, when lodged in wooden cases, became nearly half destroyed.
It has been recommended to line powder magazines with lead, as a
mean for preserving the powder from dampness. The lead, it seems, so
far attracts moisture, as to condense it. In the last volume of the
_Transactions of the American Philosophical Society_, is a memoir
on _leaden_ cartridges, by Wm. Jones, Esq. the late secretary of
the navy, which, besides preserving the powder, has advantages over
either paper or flannel. See Magazine.
What is termed the _analysis of gunpowder_, is nothing more than the
separation of its component parts, and determining the relative
proportions of its respective ingredients. We may indeed examine
the quality of the nitrate of potassa, by dissolving a portion of
powder in distilled water, and employing the reagents mentioned under
the head of nitre; but for the purpose of separating, as well as
determining the proportion of saline matter, charcoal and sulphur,
it may be readily accomplished in the following manner: Take a given
quantity of gunpowder and affuse it in distilled water sufficient
to dissolve the salt; after suffering it to remain for some time,
applying heat to assist the solution, decant the whole upon a filter
of unsized paper. The saltpetre and other saline matter will pass
through, and the sulphur and charcoal remain on the filter. By
evaporating the solution to dryness, and weighing it, the quantity
of saltpetre will be found; or, after drying the mass on the filter,
and weighing it, by subtracting its weight from that of the original,
it will give the loss sustained, which of course is the saltpetre.
By exposing the mass to a heat sufficient to evaporate the sulphur,
it will be expelled; the loss sustained will indicate its quantity,
and the weight of the residue the proportion of charcoal. The sulphur
may be even separated by subjecting gunpowder itself to the action
of a well regulated heat; it will sublime, and leave the nitre and
charcoal. It takes a much higher temperature to inflame gunpowder
than is required to volatilize sulphur. The method of extracting the
nitre from damaged powder, we have already noticed. See _nitre_.
This process also depends on the solubility of the nitre, and the
insolubility of the charcoal and sulphur. Bishop Watson, in his
_Chemical Essays_, proposed the examination of gunpowder by solution
and sublimation; a process sufficiently accurate. If it should be our
object to ascertain the presence and quantity of foreign substances,
Public-domain text, read in full here on John Shaqi.
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