A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
The silver is incorporated with the gold, and at the same time the
copper is eliminated, by cupelling with sheet lead. How much sheet lead
must be used will depend partly on how much bullion is taken, partly on
how much copper it contains. Four grams of lead will do for a .5 gram
charge; and for a .3 gram charge, 3 grams may be used. But with 20 per
cent. of copper these amounts should be doubled; with 40 per cent. of
copper they should be trebled; and with over 60 per cent. of copper four
times as much lead should be used. For small buttons of gold as little
lead as may be relied on to start cupelling may be taken; the lead may
conveniently be in the form of little cups made by folding lead foil on
a piece of glass rod. With a large number of bullion assays
systematically worked and checked a simple plan would be to always use
the quantity of lead required by the alloy containing most copper which
turns up for assay. This weight, cut out of lead foil, would be kept in
stock folded into little bags ready to receive the bullion and silver.
The silver used for inquartation must, of course, be free from gold and
is best prepared by the assayer who is to use it (see p. 66). It should
not be in long strips or angular pieces likely to perforate the lead in
which it is folded. When wrapped in the lead it should be in the middle
and should make as compact a parcel as possible.
Each little parcel, as completed, should be placed on a tray in its
properly numbered compartment. Its position here should correspond to
that it will occupy in the muffle and eventually in the cupel tray. The
cupellation must be made with all the requisite precautions. A good
smooth malleable button is needed for the next operation, which is known
as flatting.
[Illustration: FIG. 45.]
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