A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
~Flatting.~--Small buttons, such as are got in assaying most gold ores,
are placed on a polished steel anvil and flattened by one or two blows
with a hammer. The flattened discs are heated to dull redness on a clean
cupel and are then ready for parting. Somewhat larger buttons may be
similarly treated, but they should be annealed (_i.e._ heated to redness
and allowed to cool) during the flattening. The silver-gold alloy left
from the cupellation is soft and bends like lead; but after hammering or
rolling it becomes harder, gets a spring in it like a piece of
mainspring and cracks or splits somewhat easily. There should be no
cracks or stripping or even roughness on the flattened metal, since such
defects may cause the loss of small particles either during the
flattening or in the subsequent treatment with acid. The softness of the
metal is restored by heating. In bullion assays the flatting of the
buttons requires care and practice for its skilful working. The strips
of alloy for parting should be of uniform thickness and condition so
that the action of the acid shall be equal in all cases. The button is
taken from the cupel, cleaned and placed on the anvil: it is then struck
a heavy blow which widens it to about 3/4 inch in diameter; this blow is
followed by two others, one a little in front, the other behind, which
lengthen the disc and give a very blunt roof-like slope to its upper
face. It should then be annealed. This may be done by putting it in a
just red-hot scorifier heated in a muffle: it very soon attains the
right heat and may then be transferred to a cold scorifier; the hot
scorifier should be put back into the muffle. The softened disc is then
taken to the rolls (Fig. 45). The rolls are loosened until the disc can
be pressed between them. Looking through the interval between them the
rolls should appear exactly parallel; if they are not, one adjusting
screw should be loosened and the other tightened until parallelism is
obtained. The rolls are now turned and the disc should be drawn through
without any great effort. Beginners are apt to err by trying to do too
much with one turn of the handle. It is easy to stop whilst the rolls
are only just gripping the metal and then to bring the disc back by
reversing the action. If the disc was originally level and the rolls
are parallel, the metal will appear as a strip which has been merely
lengthened. If the rolls are tighter on one side the strip will be
bowed; the tighter side will correspond with the outer curve of the
crescent. A mistake of this kind may be amended by passing the strip
through the rolls the other way, so as to reverse the irregularity and
so straighten the strip. The screw on the looser side should then be
tightened until parallelism is obtained; after which more care should be
taken to tighten the two screws equally. The rolling should be stopped
when the strip is 3 or 4 inches long and of the thickness of an ordinary
visiting card.
Public-domain text, read in full here on John Shaqi.
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