A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
A scorifier is essentially a roasting dish sufficiently thick to resist,
for a time, the corrosive action of the fused metallic oxides it is to
contain. The essential property of a cupel is, that it is sufficiently
porous to allow the fused oxide to drain into it as fast as it is
formed. It should be large enough to absorb the whole of the liquid; and
of course must be made of a material upon which the liquid has no
corrosive action. Cupels do not bear transport well; hence the assayer
generally has to make them, or to supervise their making. A quantity of
bone ash is carefully mixed with water so that no lumps are formed, and
the mixture is then worked up by rubbing between the hands. The bone ash
is sufficiently wet when its cohesion is such that it can be pressed
into a lump, and yet be easily crumbled into powder. Cupel moulds should
be purchased. They are generally made of turned iron or brass. They
consist of three parts (1) a hollow cylinder; (2) a disc of metal; and
(3) a piston for compressing the bone ash and shaping the top of the
cupel. The disc forms a false bottom for the cylinder. This is put in
its place, and the cylinder filled (or nearly so) with the moistened
bone ash. The bone ash is then pressed into shape with the piston, and
the cupel finished with the help of three or four smart blows from a
mallet. Before removing the piston, turn it half-way round upon its axis
so as to loosen and smooth the face of the cupel. The cupel is got out
by pressing up the disc of metal forming the false bottom; the removal
is more easily effected if the mould is somewhat conical, instead of
cylindrical, in form. The cupels are put in a warm place to dry for two
or three days. A conveniently sized cupel is 1-1/4 inches in diameter
and about 3/4 inch high. The cavity of the cupel is about 1/4 inch deep,
and something of the shape shown in fig. 5.
[Illustration: FIG. 6.]
[Illustration: FIG. 7.]
[Illustration: FIG. 8.]
There are two kinds of furnaces required, the "wind" and "muffle"
furnaces. These are built of brick, fire-brick, of course, being used
for the lining. They are connected with a chimney that will provide a
good draught. Figure 6 shows a section of the wind furnace, fig. 7 a
section of the muffle furnace, and fig. 8 a general view of a group
comprising a muffle and two wind furnaces suitable for general work.
When in operation, the furnaces are covered with iron-bound tiles. The
opening under the door of the muffle is closed with a loosely fitting
brick. The floor of the muffle is protected with a layer of bone-ash,
which absorbs any oxide of lead that may be accidentally spilt. The fire
bars should be easily removable.
Few tools are wanted; the most important are some cast-iron moulds,
tongs (fig. 9), stirrers for calcining (fig. 10), and light tongs of a
special form for handling scorifiers and cupels (_see_ SILVER).
[Illustration: FIG. 9.]
[Illustration: FIG. 10.]
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