A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
The crucible is removed from the muffle with the tongs and carried to
the desiccator. It is best, in an office, to have a large desiccator
permanently fixed alongside the balance, into which all substances may
be put before being weighed. The substance is removed from the bench or
muffle in the small hand apparatus generally sold, and carried to the
balance room to be transferred to the large desiccator, where it is
allowed to become thoroughly cold before being weighed. Twenty minutes
is generally the time allowed after ignition before it is advisable to
weigh. Bodies allowed to cool in the air after they have been ignited will
absorb moisture, and hot bodies placed in the balance-pan will disturb
the equilibrium and show false results. Compounds that absorb moisture
must be weighed quickly; they should, therefore, be weighed in covered
vessels. Such compounds are detected by their continually-increasing
weight. They should be ignited and weighed again
in a well-covered dish.
Substances that have been washed with alcohol, ether, or any readily
volatile liquid are dried in the water oven. They quickly dry if there
is no water present, and are generally fit for weighing in less than one
hour. Sometimes drying for a few minutes only will be sufficient.
The weight of the crucible and precipitate having been obtained, the
weight of the crucible and ash is deducted; for example--
Crucible and precipitate 10.183 grams.
Crucible and ash 9.527 "
------
0.656 "
The weight of the ash is best added to that of the crucible. The amount
of ash in filter-papers must not be neglected, although papers are now
made almost free from ash, and the amount to be deducted is found by
taking eight or ten papers and burning them until they become white, and
then weighing the ash. The amount varies from 0.004 to 0.0005 gram for
different papers. Having determined the ash, place in the balance-drawer
three of the filter-papers pinned together, with the weights marked on
them in the way shown in fig. 24, so as to be readily seen when there is
occasion to refer to them.
[Illustration: FIG. 24.]
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