A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
Weights of less than 0.01 gram are generally present in a box, but it is
much more convenient to work with a rider. This is a piece of wire which
in the pan weighs 0.01 gram; it is made in such a form that it will ride
on the beam, and its effective weight decreases as it approaches the
centre. If the arm of the beam is divided into tenths, then each tenth
counting from the centre outward equals 0.001 gram or 1 milligram, and
if these tenths be further subdivided the fractions of a milligram are
obtained; and these give figures in the fourth place of decimals. A
fairly good balance should be sensitive to 0.0001 gram. The weights must
never be touched with the fingers, and the forceps for moving them is
used for no other purpose. When not in actual use the box is kept
closed. The weights must not be allowed to remain on the pan of the
balance. The balance-case must not be open without some reason. It must
be fixed level, and, once fixed, must not be needlessly moved. The bench
on which it stands should be used for no other purpose, and no one
should be allowed to lean upon it.
[Illustration: FIG. 25.]
When using a balance sit directly in front of it. Ordinarily the
substance to be weighed is best put on the pan to the user's left; the
weights and the rider are then easily manipulated. Powders, &c., should
not be weighed directly on the balance; a counterpoised watch-glass or
metal scoop (fig. 25) should be used. In some cases it is advisable to
use a weighing-bottle. This is a light, well-stoppered bottle (fig. 3)
containing the powdered ore. It is first filled and weighed; then some
of the substance is carefully poured from it into a beaker or other
vessel, and it is weighed again; the difference in the two weighings
gives the weight of substance taken. A substance must always be cold
when weighed, and large glass vessels should be allowed to stand in the
balance-box a little while before being weighed. Always have the balance
at rest when putting on or taking off anything from the pans. Put the
weights on systematically. In using the rider (except you have a reason
to the contrary), put it on at the 5; if this is too much, then try it
at the 3; if then the weights are too little, try at the 4, if still not
enough, the correct weight must be between the 4 and 5; try half-way
between.
It is best to work with the balance vibrating; equilibrium is
established when the vibration to the left is the mean of the preceding
and succeeding vibrations to the right. For example, if it vibrates 6
divisions to the right on one swing, and 5 divisions on the next, the
intermediate vibration to the left should have been 5-1/2.
Note whether the substance increases in weight whilst on the balance. If
it does it may be because it was put on warm, and is cooling, or it may
be because it is taking up moisture from the air. Substances which take
up moisture rapidly should be weighed in clipped watch-glasses or in
light-weighing bottles or tubes.
Public-domain text, read in full here on John Shaqi.
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