A Text-book of Paper-makingCross, C. F. (Charles Frederick)
Science
A Text-book of Paper-making
Cross, C. F. (Charles Frederick)
Paper industry; Papermaking
It is essential in dissolving the recovered soda that a high
temperature should be employed, as otherwise a portion of the soda
present as silicate of soda will be lost, as it is only with difficulty
soluble, and requires rather prolonged heating with water. Whatever the
form of apparatus employed it should be so arranged that, after running
off the strong liquor, the insoluble residue may be further treated
with water. In the case of the vats mentioned above, this process
is made continuous, pure water being run in at one end, and strong
liquor flowing from the other. If other forms are used, the liquor
after settling, may be run off by means of a pipe passing through the
bottom or side of the vessel, and near the bottom, and consisting of
two parts, one long, and one short. The short part is stationary, and
is connected to the longer part by means of a movable knee joint,
allowing it to be deflected. The liquor having settled sufficiently,
the movable limb is lowered beneath the surface of the liquor which is
then allowed to flow through. As the surface of the liquor falls, the
pipe is gradually lowered. In this way the clear solution can be run
off without disturbing the residue at the bottom. The open end of the
pipe is usually covered with coarse wire gauze, to keep back insoluble
impurities. With properly calcined recovered soda, the solution should
be bright and almost colourless. If at all brown in colour, and if
it has an empyreumatic odour, it indicates imperfect calcination.
The residue in the dissolving tanks consists chiefly of carbonaceous
matter, together with some soda, insoluble matter, &c.
The liquor is now ready to be causticised. This should be done in a
separate vessel, although it is the practice in many mills to perform
this operation in the same vessel in which the solution of the soda
has been conducted. A good form of causticiser can be made from an old
egg-shaped boiler, by cutting it in two along its length. {189}
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