Wax 32.00
Resino-extractive 5.00
Black powder 15.00
Kernels 47.00
------
99.50
Loss .50
------
100.00
The chemical properties of the wax and of the black powder may be
made the subject of another communication.
_Earthy phosphate of iron_ has recently been found at Hopkinton,
Mass. It exists there in large quantities, and is employed as
a pigment. The gentleman on whose grounds it was found sent me
several pounds of it.
J. F. D.
ART. XVI. _Analysis of Wacke, by Dr._ J. W. WEBSTER, _of Boston_.
One hundred parts exposed to a red heat in a platina crucible lost
18.5, acquired an umber brown colour, and a degree of hardness
sufficient to scratch glass.
One hundred parts reduced to fine powder were mixed with four
times the weight of soda, and exposed to heat, gradually increased
for three quarters of an hour; at the expiration of which time,
the whole had acquired a pasty consistence. The crucible was now
removed from the fire, its outer surface carefully wiped. Muriatic
acid was poured on till all effervescence ceased. The solution
obtained was evaporated to dryness, gradually assuming an orange
red colour. Water was now poured upon the mass, after which it was
filtered, and the powder remaining carefully dried; after ignition,
and while warm, it weighed 28 parts. This powder was insoluble in
muriatic acid, and of a white colour.
To the filtered solution, reduced by evaporation, carbonate of
potash was added, the precipitate was collected on a filter, washed
and dried; it weighed 23 parts. This powder was redissolved in
sulphuric acid, sulphate of potash added, and crystals of alum
finally obtained; hence this powder was alumine. To the liquor from
which the silex and alumine had thus been separated, acetic acid
was added; the whole evaporated to dryness; the excess of acid
being removed, a small quantity of water was poured on, and after
strong ignition, the precipitate weighed 4.5.
Into a very small tubulated retort I introduced a portion from the
same mass, whence the piece submitted to analysis was broken, and
obtained over mercury the carbonic acid in the usual manner. This
was equal to 2.32; by deducting this from 18.5 the loss during
exposure to red heat, we shall have 16.18, the proportion of water.
The oxide of iron was separated from the solutions after the
addition of acetic acid, by ammonia, and weighed 26 parts.
Silex 28.
Alumine 23.
Lime 4.5
Carbonic acid 2.32
Water 16.18
Oxide of iron 26.
------
100
AGRICULTURE AND ECONOMICS.
ART. XVII. _On the Comparative Quantity of Nutritious Matter which
may be obtained from an Acre of Land when cultivated with Potatoes
or Wheat, by Dr._ ELI IVES, _Professor of Materia Medica and Botany
in Yale College_.
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