An Introductory Course of Quantitative Chemical Analysis: With Explanatory NotesTalbot, Henry Paul
Science
An Introductory Course of Quantitative Chemical Analysis: With Explanatory Notes
Talbot, Henry Paul
Chemistry, Analytic -- Quantitative
If a filter paper is folded along its diameter, and again folded along
the radius at right angles to the original fold, a cone is formed on
opening, the angle of which is 60°. Funnels for analytical use are
supposed to have the same angle, but are rarely accurate. It is
possible, however, with care, to fit a filter thus folded into a
funnel in such a way as to prevent air from passing down between the
paper and the funnel to break the column of liquid in the stem,
which aids greatly, by its gentle suction, in promoting the rate of
filtration.
Such a filter has, however, the disadvantage that there are three
thicknesses of paper back of half of its filtering surface, as a
consequence of which one half of a precipitate washes or drains more
slowly. Much time may be saved in the aggregate by learning to fold a
filter in such a way as to improve its effective filtering surface.
The directions which follow, though apparently complicated on first
reading, are easily applied and easily remembered. Use a 6-inch filter
for practice. Place four dots on the filter, two each on diameters
which are at right angles to each other. Then proceed as follows:
(1) Fold the filter evenly across one of the diameters, creasing it
carefully; (2) open the paper, turn it over, rotate it 90° to the
right, bring the edges together and crease along the other diameter;
(3) open, and rotate 45° to the right, bring edges together, and
crease evenly; (4) open, and rotate 90° to the right, and crease
evenly; (5) open, turn the filter over, rotate 22-(1/2)° to the right,
and crease evenly; (6) open, rotate 45° to the right and crease
evenly; (7) open, rotate 45° to the right and crease evenly; (8) open,
rotate 45° to the right and crease evenly; (9) open the filter, and,
starting with one of the dots between thumb and forefinger of the
right hand, fold the second crease to the left over on it, and do
the same with each of the other dots. Place it, thus folded, in the
funnel, moisten it, and fit to the side of the funnel. The filter will
then have four short segments where there are three thicknesses
and four where there is one thickness, but the latter are evenly
distributed around its circumference, thus greatly aiding the passage
of liquids through the paper and hastening both filtration and washing
of the whole contents of the filter.
!SAMPLE PAGES FOR LABORATORY RECORDS!
!Page A!
Date
CALIBRATION OF BURETTE No.
Public-domain text, read in full here on John Shaqi.
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