Balkan Peninsula -- Description and travel; Eastern question (Balkan)
“Otto-of-rose, when analysed, is found to consist of two ingredients:
the oleoptene, which is the liquid and odoriferous part of the
otto-of-rose, and the stereoptene, which is the solid and odourless
part, and causes the crystallisation of the otto-of-rose. The proportion
in which these two ingredients are combined in the pure otto-of-rose is
more or less fixed, varying only from 10 to 15 per cent. according to
the elevation of the localities in which the otto is produced. The
highest proportion—15 per cent.—is found in otto-of-rose distilled in
villages situated highest in the Balkans; while the villages down in the
plains produce otto-of-rose containing only 10 to 11 per cent. of
stereoptene. We have lately made experiments to distil these two
ingredients separately, but they can best be separated from each other
by a very simple physical process. The average proportion of these two
ingredients in our stocks during the last five years has been about 12½
per cent. of stereoptene and 87½ per cent. of oleoptene.
“The oil usually employed for the adulteration of otto-of-rose is the
geranium oil (_Palagonium Radula_) known to the trade as Turkish
geranium oil. This oil is made in India and is sold in Constantinople.
Formerly they used this oil as adulterant in its crude state, but now it
is generally refined in rose-water or rose-flower before it is used. No
matter how well refined, it is impossible to put 5 per cent. of it in
otto-of-rose without changing the freezing point of the otto, its
specific gravity, and the proportion in which the stereoptene and
oleoptene are combined. Geranium oil contains no stereoptene, and in
consequence does not crystallise. In the best refined geranium oil the
specific gravity is fully ·880—a difference in weight of about eighteen
points. All this helps to detect its presence in otto-of-rose. It can
also be detected by means of the iodine as well as the nitric acid
tests. The presence of geranium oil in otto-of-rose lowers its freezing
point, renders its specific gravity heavier, and changes the proportion
in which the oleoptene and stereoptene are combined.
[Illustration: The Rose-fields near Kazanlik.]
“In order to rectify these defects, the use of spermaceti, paraffin, and
alcohol have often been resorted to, but the presence of all these three
substances can be discovered without any difficulty. The crystals of
both spermaceti and paraffin are entirely different from the crystals of
the stereoptene of otto-of-rose, and otto-of-rose containing any
proportion of either will lose, when congealed, its sharp-pointed,
needle-like crystals. Besides, paraffin and spermaceti being fatty oils,
are much heavier, and in time will settle at the bottom. Furthermore,
they are not volatile as stereoptene. The presence of alcohol is
detected either by the use of double distilled water or of pure
glycerine.”
Public-domain text, read in full here on John Shaqi.
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