Extraction in open vats is used both for skin and bone gelatine. It is
usually preferred when it is intended to extract at the lower
temperatures, and it is usually adopted also when the material is such
that the extraction is comparatively rapid, as for example in the case
of skin gelatine and bones by the acid process. The vats themselves are
often constructed of wood, in which case they are heated by a copper (or
brass) steam coil. They may be constructed also of iron, cast or
wrought, the former being cheaper, less liable to corrosion, but more
liable to fracture. In the case of iron vessels the heating may also be
done by a steam coil beneath a false bottom, but it is sometimes
arranged that iron vats are heated by a steam jacket, and even by a
hot-water jacket. Heating in either wood or iron vessels has been
brought about by direct application of raw steam, but the results are
both uncertain and unsatisfactory owing to local overheating. Whatever
appliances are used agitation of the material or liquor is advantageous.
Extraction in closed vats is also used. This is generally associated
with extraction at higher temperatures, and more often also with the
manufacture of glue than of gelatine. It has been used on the Continent
for skin glue, and in this country for bone gelatine and glue by the
"boiling" process. In this system of working the vessels are usually
made of 3/8-inch steel plates, and will take a charge of 3 to 5 tons of
material. It is claimed for the system that there is a lessened steam
consumption as well as lesser manipulation, that strong liquors are more
easily and quickly obtained, and that the material may be more
thoroughly exhausted. Extraction is sometimes made by steam and water
playing alternately on the material, but many manufacturers prefer the
use of direct steam, keeping the pressure at 15 lbs. for about 2 hours.
The pressure is then reduced considerably and the process finished off
by spraying the material with water. From such a procedure a 20 per
cent. glue sol may be obtained. It is common to work such extractors in
couples or in batteries of four to six. It will be readily understood
that the process is suitable for making bone glue when the phosphate has
not been dissolved. The high temperature is in this case almost
necessary to ensure thorough extraction. It will be equally clear that
the process is not so suitable in the manufacture of a strong gel.
As alternatives to the systems of fractional extraction, several
processes have been devised in which the extraction is continuous.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account