The next stage in clarification is the separation of precipitated
matters and of the coalesced particles of grease. This may be attained
by the two processes usual in such a problem of chemical engineering,
viz. sedimentation and filtration. After precipitation, therefore, the
sol should be allowed to stand for some hours, during which time the
precipitate not only flocculates but also settles to the bottom, and the
globules of grease coalesce further and rise to the top, from which they
may be skimmed off. Sedimentation alone is both too slow and too
incomplete to be sufficient for proper clarification, and in these days
it is always supplemented by the use of the filter-press. This
well-known appliance can easily be adapted to the local requirements of
the manufacturer. As speed of working is an essential requirement it is
necessary to have a large filtering surface, and this may be done either
by increasing the number of plates in the press or by increasing the
area of the plates used. The large plates, however, are often cumbrous
and inconvenient, and if of metal are very heavy. The plates may be
constructed of well-seasoned wood, or in the case of alkaline gelatine
and glues, even of iron. The framework is in any case usually iron. Acid
gelatines and glues may have wooden plates, but "acid-proof" alloys are
sometimes used to make them. Where it is essential to filter quickly two
presses may be arranged _in parallel_, thus doubling the active
filtering surface. When it is essential to obtain the highest possible
clarity, two presses may be worked _in series_, which, in effect, means
that the sol is filtered twice. In using the filter press for gelatine
and glue it is most necessary to observe the most scrupulous
cleanliness, and the plates must be frequently washed and sterilized.
Rideal recommends weak chlorine water or bleaching powder solution for
this purpose.
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