A great stride forward was made by Howard's invention of the Vacuum Pan.
This made it possible to undertake concentration at much lower
temperatures, a most important improvement in the case of gelatine and
other organic matters easily damaged by heat. The process, however, was
still slow, and the sol exposed to heat for a long time, as must be the
case when evaporation takes place in bulk. These disadvantages were
still fatal to the production of the highest-grade gelatine. There were
also the practical difficulties of entrainment ("blowing over"), in
which parts of the sol were carried away by the escaping vapour, and
also of "incrustation" which so rapidly reduces the heating efficiency
and evaporative capacity of the machine. The vacuum pan, however,
presented two decided advantages--evaporation at a low temperature, and,
as a corollary, the possibility of utilizing exhaust steam to attain
this temperature.
Whilst the vacuum pan was a satisfactory machine for many branches of
chemical engineering, the problem of evaporation was still unsolved for
gelatine liquor because of the "stewing" involved, until the advent of
the "film evaporator," which dealt with the liquor not in bulk, but in a
continuous stream. In this way the product was only exposed to heat for
a comparatively short time. Many evaporators of this type came into
being, and rapid improvement was made in the constructional details. The
film evaporators retained usually the advantage of evaporation _in
vacuo_, so that it was now possible to evaporate gelatine sols by
exposure for a short time to a comparatively low temperature. Of this
type of evaporator, the Lillie, Yaryan, Schwager, Claassen, Greiner,
Blair Campbell, and the Kestner machines are well-known examples.
A further advance in solving this problem was the application of the
principle of multiple-effect evaporation. The vapour driven off during
evaporation possesses of course many heat units, and is of very
considerable volume. In multiple-effect evaporators this vapour is used
to work a similar evaporator, and the evaporated liquor passes
immediately into what is practically a second machine, and is further
evaporated by the heat from the vapour just driven from it. Such an
arrangement would be termed a double-effect evaporator. The vapour from
the second effect may of course be similarly used to operate a third
effect, and the vapour from this to work a fourth effect, and so on.
Thus, we may have triple effect, quadruple effect, etc., even up to
octuple effect. The great advantage of multiple-effect evaporation is in
the saving of costly steam. Reavell gives the following figures to
illustrate the economy thus obtained:--
WATER EVAPORATED PER 100 UNITS STEAM.
Public-domain text, read in full here on John Shaqi.
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