Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume ICooley, Arnold James
Science
Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume I
Cooley, Arnold James
Formulas, recipes, etc.; Industrial arts -- Dictionaries; Technology -- Dictionaries
2. From BONE-LIQUOR, &c.[50]——The ammoniacal liquor technically called
‘bone-liquor’ or ‘bone-spirit,’ and formerly known under the name of
‘spirit of hartshorn,’ is essentially a solution of carbonate of ammonia
more or less contaminated with volatile empyreumatic oil. Its conversion
into SAL AMMONIA may be easily effected by saturating it with hydrochloric
acid, evaporating the resulting neutral solution in lead or iron boilers
until a pellicle begins to form, then pumping or running off the hot
liquors into the crystallisers, and, lastly, draining and drying the
crystals. The salt thus obtained may be purified either by sublimation or
by recrystallisation. The whole series of processes closely resemble those
already described, except in being less troublesome, owing to the absence
of the tarry and other foreign matters which impede and complicate them
when gas-liquor is employed.
[Footnote 50: That employed in England is chiefly obtained, as already
mentioned, from the manufacturers of bone-black or animal charcoal; but,
on the Continent, the liquor obtained by a like destructive distillation
of various animal offals (blood, flesh, horn, hoofs, woollen rags and
waste, hair, scrapings of hides, leather cuttings, &c.) is employed for
the same purpose. The preparatory process by which this liquor is obtained
is essentially the same in each case; except that with animal offal the
temperature should not exceed a red-brown heat, in order that the
resulting charcoal may afterwards serve to make ferrocyanide of potassium
and Prussian blue. These liquors have usually a density ranging between 8°
and 9° Baumé (Ure; = sp. gr. 1·056 to 1·063).]
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