Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
Distillation, as hath been already said, is an operation by which
we separate from a body, by the help of a gradual heat, the several
principles of which it consists.
There are three methods of distilling. The first is performed by
applying the heat over the body whose principles are to be extracted.
In this case, as the liquors, when heated and converted into vapours,
constantly endeavour to fly from the center of heat, they are forced to
re-unite in the lower part of the vessel, that contains the matter in
distillation, and so passing through the pores or holes of that vessel,
they fall into another cold vessel applied underneath to receive them.
This way of distilling is on this account called distilling _per
Descensum_. It requires no other apparatus than two vessels figured
like segments of hollow spheres, whereof that which is pierced with
little holes, and intended to contain the matter to be distilled,
should be much less than the other, which is to contain the fire,
and to fill its aperture exactly; the whole together to be supported
vertically upon a third vessel, which is to serve the purpose of a
recipient, admitting into its mouth the convex bottom of the vessel
containing the matter to be distilled, which must accurately fill it.
This method of distilling is but little used.
The second method of distilling is performed by applying the heat
underneath the matter to be decomposed. On this occasion the liquors
being heated, rarefied, and converted into vapours, rise, and are
condensed in a vessel contrived for that purpose, which we shall
presently describe. This way of distilling is called distilling _per
Ascensum_, and is much used.
The vessel in which this distillation _per Ascensum_ is performed we
call an _Alembic_.
There are several sorts thereof, differing from one another both in the
matter of which, and the manner in which, they are made.
Those employed to draw the odoriferous waters and essential oils of
plants are generally made of copper, and consist of several pieces. The
first, which is designed to contain the plant, is formed nearly like a
hollow cone, the vertex whereof is drawn out in the shape of a hollow
cylinder or tube: this part is named the _Cucurbit_, and its tube the
_Neck_ of the _Alembic_. To the upper end of this tube another vessel
is soldered: this is called the _Head_, and commonly has likewise the
form of a cone, joined to the neck of the alembic by its base, round
which, on the inside, is hollowed a small groove, communicating with
an orifice that opens at its most depending part. To this orifice is
soldered a small pipe in a direction sloping downwards, which is called
the _Nose_, _Spout_, or _Beak_ of the alembic.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account