Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
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Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
It is moreover proper to have, in a laboratory, sundry retorts with
necks of different diameters. Wide necks will be found the fittest
for conveying thick matters, and such as readily become fixed; for
instance, some very thick fetid oils, butter of antimony, _&c._; for
as these matters acquire a consistence as soon as they are out of
the reach of a certain degree of heat, they would soon choak a narrow
neck, and by stopping the vapours which rise at the same time from the
retort, might occasion the bursting of the vessels.
Some retorts are also made with an opening on their upper side, like
that of tubulated glass alembics, which is to be closed in the same
manner with a glass stopple. These retorts are also called Tubulated
retorts, and ought always to be used whenever it is necessary to
introduce fresh matter into the retort during the operation; seeing it
may be done by means of this invention, without unluting and reluting
the vessels; which ought always to be avoided as much as possible.
One of the things that most perplexes the Chymists, is the prodigious
elasticity of many different vapours, which are frequently discharged
with impetuosity during the distillation, and are even capable of
bursting the vessels with explosion, and with danger to the artist. On
such occasions it is absolutely necessary to give these vapours vent,
as we shall direct in its proper place: but as that can never be done
without losing a great many of them; as some of them in particular
are so elastic that scarce any at all would remain in the vessel; for
instance, those of the spirit of nitre, and especially those of the
smoking spirit of salt; the practice is to make use of very large
receivers, of about eighteen or twenty inches diameter, that the
vapours may have sufficient room to circulate in, and by applying to
the wide surface presented them by the extensive inside of such a large
vessel, may be condensed into drops. These huge receivers are commonly
in the form of hollow globes, and are called Ballons.
To give these vapours still more room, ballons have been contrived
with two open gullets in each, diametrically opposite to one another;
whereof one admits the neck of the retort, and the other is received by
one of the gullets of a second ballon of the same form, which is joined
in like manner to a third, and so on. By this artifice the space may be
enlarged at pleasure. These ballons with two necks are called Adopters.
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