Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
It is easy to imagine, that such a vessel must be much lower than
the alembic. It is indeed no more than a hollow globe, whose upper
part degenerates into a neck or tube, that is bent into a horizontal
position; for which reason this instrument is called a _Retort_: it is
always of one single piece.
The matter to be distilled is introduced into the body of the retort by
means of a ladle with a long tubular shank. Then it is set in a furnace
built purposely for this use, and so that the neck of the retort coming
out of the furnace may, like the nose of the alembic, stand in a
sloping position, to facilitate the egress of the liquors, which by its
means are conveyed to a receiver, into which it is introduced, and with
which it is luted. This way of distilling, in which the vapours seem
rather to be driven out of the vessel horizontally and laterally, than
raised up and sublimed, is for that reason called Distillation _per
Latus_.
Retorts are, of all the instruments of distillation, those that must
sustain the greatest heat, and resist the strongest solvents; and
therefore they must not be made of metal. Some, however, which are
made of iron may do well enough on certain occasions: the rest are
either of glass or earth. Those of glass, for the reasons above given,
are preferable to the other sort, in all cases where they are not to
be exposed to such a force of fire as may melt them. The best glass,
that which stands both heat and solvents best, is that in which there
are fewest alkaline salts. Of this sort is the green German glass: the
beautiful white crystal glass is far from being equally serviceable.
Retorts, as well as alembics, may be of different forms. For example,
some matters are apt to swell, and rise over the neck of the retort in
substance, without suffering any decomposition; when such matters are
to be distilled in a retort, it is proper that the body of the vessel,
instead of being globular, be drawn out into the form of a pear, so as
nearly to resemble that of a cucurbit. In a retort of this kind, the
distance between the bottom and the neck being much greater than in
those whose bodies are spherical, the matters contained have much more
room for expansion; so that the inconvenience here mentioned is thereby
prevented. Retorts of this form are called English retorts. As they
hold the middle place between alembics and common retorts, they may be
used to distil such matters as have a mean degree of volatility between
the greatest and the least.
Public-domain text, read in full here on John Shaqi.
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