Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
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Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
To prevent this inconvenience, it is necessary that in every receiver
there be a small hole, which being stopped only with a little lute may
easily be opened and shut again as occasion requires. It serves for a
vent-hole to let out the vapours, when the receiver begins to be too
much crowded with them. Nothing but practice can teach the artist when
it is requisite to open this vent. If he hits the proper time, the
vapours commonly rush out with rapidity, and a considerable hissing
noise; and the vent should be stopped again as soon as the hissing
begins to grow faint. The lute employed to stop this small hole ought
always to be kept so ductile, that, by taking the figure of the hole
exactly, it may entirely stop it. Besides, if it should harden upon the
glass, it would stick so fast that it would be very difficult to remove
it without breaking the vessel. This danger is easily avoided by making
use of the fat lute, which continues pliant for a long time, when it is
not exposed to an excessive heat.
This way of stopping the vent-hole of the receiver has yet another
advantage: for if the hole be of a proper width, as a line and half, or
two lines, in diameter, then, when the vapours are accumulated in too
great a quantity, and begin to make a great effort against the sides of
the receiver, they push up the stopple, force it out, and make their
way through the vent-hole: so that, by this means, the breaking of the
vessels may always be certainly prevented. But great care must be taken
that the vapours be not suffered to escape in this manner, except when
absolute necessity requires it; for it is generally the very strongest
and most subtile part of a liquor which is thus dissipated and lost.
Heat being the chief cause that puts the elasticity of the vapours in
action, and prevents their condensing into a liquor, it is of great
consequence in distillation that the receiver be kept as cool as
possible. With this view a thick plank should be placed between the
receiver and the body of the furnace, to intercept the heat of the
latter, and prevent its reaching the former. As the vapours themselves
rise very hot from the distilling vessel, they soon communicate their
heat to the receiver, and especially to its upper part, against which
they strike first. For this reason it is proper that linen cloths, dipt
in very cold water, be laid over the receiver, and frequently shifted.
By this means the vapours will be considerably cooled, their elasticity
weakened, and their condensation promoted.
By what hath been said in this first part, concerning the properties
of the principal agents in Chymistry, the construction of the most
necessary vessels and furnaces, and the manner of using them, we are
sufficiently prepared for proceeding directly to the operations,
without being obliged to make frequent and long stops, in order to give
the necessary explanations on those heads.
Public-domain text, read in full here on John Shaqi.
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