Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
A few slips of paper applied round the neck of the vessels with common
size will be sufficient to keep in such vapours as are aqueous or not
very spirituous.
If the vapours are more acrid, or more spirituous, recourse may be had
to slips of bladder long steeped in water, which containing a sort of
natural glue, close the junctures of the vessels very well.
If it be required to confine vapours of a still more penetrating
nature, it will be proper to employ a lute that quickly grows very
hard; particularly a paste made with quick-lime and any sort of jelly,
whether vegetable or animal; such as the white of an egg, stiff size,
_&c._ This is an excellent lute, and not easily penetrated. It is also
used to stop any cracks or fractures that happen to glass vessels. But
it is not capable of resisting the vapours of mineral acid spirits,
especially when they are strong and smoking: for that purpose it is
necessary to incorporate the other ingredients thoroughly with fat
earth softened with water; and even then it frequently happens that
this lute is penetrated by acid vapours, especially those of the spirit
of salt, which of all others are confined with the greatest difficulty.
In such cases its place may be supplied with another, which is called
Fat Lute, because it is actually worked up with fat liquors. This
lute is composed of a very fine cretaceous earth, called tobacco-pipe
clay, moistened with equal parts of the drying oil of lint-seed, and a
varnish made of amber and gum copal. It must have the consistence of
a stiff paste. When the joints of the vessels are closed up with this
lute, they may, for greater security, be covered over with slips of
linen smeared with the lute made of quick-lime and the white of an egg.
Chymical vessels are liable to be broken in an operation by other
causes besides the sudden application of heat or cold. It frequently
happens, that the vapours of the matters exposed to the action of fire
rush out with such impetuosity, and are so elastic, that, finding no
passage through the lute with which the joints of the vessels are
closed, they burst the vessels themselves, sometimes with explosion and
danger to the operator.
Public-domain text, read in full here on John Shaqi.
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