Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
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Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
Take any quantity of nitrous earths or stones; reduce them to powder;
and therewith mix a third part of the ashes of green-wood and
quick-lime. Put this mixture into a barrel or vat, and pour on it hot
water to about twice the weight of the whole mass. Let it stand thus
for twenty-four hours, stirring it from time to time with a stick. Then
filter the liquor through brown paper, or pass it through a flannel
bag, till it come clear: it will then have a yellowish colour. Boil
this liquor, and evaporate till you perceive that a drop of it let fall
on any cold body coagulates. Then stop the evaporation, and set your
liquor in a cool place. In the space of four and twenty hours crystals
will be formed in it, the figure of which is that of an hexagonal
prism, having its opposite planes generally equal, and terminated at
each extremity by a pyramid of the same number of sides. These crystals
will be of a brownish colour, and deflagrate on a live coal.
Decant the liquor from these crystals; mix it with twice its weight
of hot water; evaporate and crystallize as before. Repeat the same
operation till the liquor will yield no more crystals: it will then be
very thick, and goes by the name of _Mother of Nitre_.
_OBSERVATIONS._
Earths and stones that have been impregnated with animal or vegetable
juices susceptible of putrefaction, and have been long exposed to the
air, but sheltered from the sun and rain, are those which yield the
greatest quantity of Nitre. But all sorts of earths and stones are not
equally fit to produce it. None is ever found in flints or sands of a
crystalline nature.
Some earths and stones abound so with Nitre, that it effloresces
spontaneously on their surface, in the form of a crystalline down. This
Nitre may be collected with brooms, and accordingly has the name of
_Salt-petre Sweepings_. Some of this sort is brought from India.
Hitherto we are much in the dark as to the origin and generation of
Nitre. Some Chymists pretend that the Nitrous Acid is diffused through
the air, and gradually deposited in such earths and stones as are
qualified to receive it.
Others, considering that none of it is ever obtained but from earths
that have been impregnated with vegetable or animal juices, have from
thence concluded those two kingdoms to be the general repositories
of the Nitrous Acid; that if we do not perceive it to exist in such
matters at all, or at least in any great quantity, till they have
undergone putrefaction, and are in some measure incorporated with
suitable earths and stones, it is because the Acid is so entangled
with heterogeneous particles that it requires the assistance of
putrefaction, and much more of filtration through an earth, to
disengage it, and enable it to appear in its proper nature.
Public-domain text, read in full here on John Shaqi.
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