Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
Having put the Gold you intend to purify into a crucible, set it in
a melting furnace, cover it, and make the Gold flow. When the metal
is in fusion cast upon it, by a little at a time, twice its weight
of pure crude Antimony in powder, and after each projection cover
the crucible again immediately: this done keep the matter in fusion
for a few minutes. When you perceive that the metallic mixture is
perfectly melted, and that its surface begins to sparkle, pour it out
into a hollow iron cone, previously heated, and smeared on the inside
with tallow. Immediately strike with a hammer the floor on which the
cone stands; and when all is cold, or at least sufficiently fixed,
invert the cone and strike it: the whole metallic mass will fall out,
and the under part thereof, which was at the point of the cone, will
be a Regulus more or less yellow as the Gold was more or less pure.
On striking the metallic mass the Regulus will freely part from the
sulphureous crust at top.
Return this Regulus into the crucible, and melt it. Less fire will do
now than was required before. Add the same quantity of Antimony, and
proceed as at first. Repeat the same operation a third time, if your
Gold be very impure.
Then put your Regulus into a good crucible, much larger than is
necessary to hold it. Set your crucible in a melting furnace, and heat
the matter but just enough to make it flow, with a smooth, brilliant
surface. When you find it thus conditioned, point towards it the nose
of a long-snouted pair of bellows, and therewith keep gently and
constantly blowing. There will arise from the crucible a considerable
smoke, which will abate greatly when you cease to blow, and increase
as soon as you begin again. You must raise the fire gradually as you
approach towards the end of the operation. If the surface of the metal
lose its brilliant polish, and seem covered with a hard crust, it is
a sign the fire is too weak; in which case it must be increased, till
the surface recover its shining appearance. At last, when no more smoke
rises, and the surface of the Gold looks neat and greenish, cast on
it, by little and little, some pulverized Nitre, or a mixture of Nitre
and Borax. The matter will swell up. Continue thus adding more Nitre
gradually, till no commotion is thereby produced in the crucible; and
then let the whole cool. If you find, when the Gold is cold, that it is
not tough enough, melt it over again; when it begins to melt, cast in
the same Salts as before; and repeat this till it be perfectly ductile.
_OBSERVATIONS._
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account